Spectral study of a new dihydroisocoumarin
文献类型：期刊论文
| 作者 | Wang, HM; Shi, W; Xu, YK; Liu, Y; Lu, MJ; Pan, JQ |
| 刊名 | MAGNETIC RESONANCE IN CHEMISTRY
 |
| 出版日期 | 2003-09-01 |
| 卷号 | 41期号:9页码:718-720 |
| 关键词 | Nmr H-1 Nmr C-13 Nmr 2d Nmr X-ray Crystallography 3 4-dihydro-6 8-dihydroxy-3-(2 '-acetyl-3 '-hydroxy-5 '-methoxy)Methyl-1h-[2]Benzopyran-1-one |
| ISSN号 | 0749-1581 |
| DOI | 10.1002/mrc.1211 |
| 英文摘要 | A novel dihydroisocoumarin, 3,4-dihydro-6,8-dihydroxy3-(2'-acetyl-3'-hydroxy-5'-methoxy)methyl-1H-[2]benzo-pyran-1-one, was isolated from the chloroform extract of the sap of the traditional herb Aloe vera. Its structure was determined by high-resolution negative fast atom bombardment mass spectrometry (MS), 2D NMR spectroscopy and x-ray crystallography. The molecular structure was elucidated by 2D NMR analysis. The complete assignment of the H-1 and C-13 NMR spectra of this compound was performed by using H-1 detected one-bond heteronuclear multiple quantum correlation (HMQC) and long-range (two and three bonds) heteronuclear multiple quantum bond correlation (HMBC) experiments. Detailed analyses of the one- and two-dimensional NMR techniques are presented in additional to the spectral properties (MS, IR and UV). Copyright (C) 2003 John Wiley Sons, Ltd. |
| 语种 | 英语 |
| WOS记录号 | WOS:000184847000011 |
| 出版者 | JOHN WILEY & SONS LTD |
| 源URL | [http://ir.iccas.ac.cn/handle/121111/80767]  |
| 专题 | 中国科学院化学研究所 |
| 通讯作者 | Liu, Y |
| 作者单位 | 1.Chinese Acad Sci, Inst Chem, State Key Lab Struct Chem Unstable & Stable Speci, Ctr Mol Sci, Beijing 100080, Peoples R China 2.Peking Univ, Ctr Anal & Measurement, Beijing 100871, Peoples R China |
| 推荐引用方式 GB/T 7714 | Wang, HM,Shi, W,Xu, YK,et al. Spectral study of a new dihydroisocoumarin[J]. MAGNETIC RESONANCE IN CHEMISTRY,2003,41(9):718-720. |
| APA | Wang, HM,Shi, W,Xu, YK,Liu, Y,Lu, MJ,&Pan, JQ.(2003).Spectral study of a new dihydroisocoumarin.MAGNETIC RESONANCE IN CHEMISTRY,41(9),718-720. |
| MLA | Wang, HM,et al."Spectral study of a new dihydroisocoumarin".MAGNETIC RESONANCE IN CHEMISTRY 41.9(2003):718-720. |
入库方式： OAI收割
来源：化学研究所
浏览0
下载0
收藏0
其他版本
除非特别说明，本系统中所有内容都受版权保护，并保留所有权利。