Determination of diterpenoid triepoxides in Tripterygium wilfordii by micellar electrokinetic capillary chromatography
文献类型：期刊论文
| 作者 | Song, XR; Yang, GL; Zhao, JX; Chen, Y; Sun, HW; Zhang, HY |
| 刊名 | PHYTOCHEMICAL ANALYSIS
 |
| 出版日期 | 2003-05-01 |
| 卷号 | 14期号:3页码:132-136 |
| 关键词 | Micellar Electrokinetic Capillary Chromatography Diterpenoid Triepoxides Tripterygium WilF.rdii Hook F. |
| ISSN号 | 0958-0344 |
| DOI | 10.1002/pca.692 |
| 英文摘要 | A micellar electrokinetic capillary chromatographic (MEKC) method has been established for the identification and determination of diterpenoid triepoxides in the Chinese herb Tripterygium wilfordii Hook F. and its preparations. Studies of the influence of boric acid and borax buffer concentration and pH, and of sodium dodecylsulphate (SDS) concentration have been carried out, and the optimum separation for the triepoxides was achieved using 20 mM boric acid and 10 mM borax with 20 mM SDS as the running buffer. MEKC was found to exhibit good accuracy, precision and repeatability. The sensitivity of the assay was sufficient to monitor the three active components in T. wilfordii and its preparations. Copyright (C) 2003 John Wiley Sons, Ltd. |
| 语种 | 英语 |
| WOS记录号 | WOS:000182913500002 |
| 出版者 | JOHN WILEY & SONS LTD |
| 源URL | [http://ir.iccas.ac.cn/handle/121111/80823]  |
| 专题 | 中国科学院化学研究所 |
| 通讯作者 | Yang, GL |
| 作者单位 | 1.Hebei Univ, Dept Chem, Baoding 071002, Peoples R China 2.Chinese Acad Sci, Inst Chem, Ctr Mol Sci, Beijing 100080, Peoples R China |
| 推荐引用方式 GB/T 7714 | Song, XR,Yang, GL,Zhao, JX,et al. Determination of diterpenoid triepoxides in Tripterygium wilfordii by micellar electrokinetic capillary chromatography[J]. PHYTOCHEMICAL ANALYSIS,2003,14(3):132-136. |
| APA | Song, XR,Yang, GL,Zhao, JX,Chen, Y,Sun, HW,&Zhang, HY.(2003).Determination of diterpenoid triepoxides in Tripterygium wilfordii by micellar electrokinetic capillary chromatography.PHYTOCHEMICAL ANALYSIS,14(3),132-136. |
| MLA | Song, XR,et al."Determination of diterpenoid triepoxides in Tripterygium wilfordii by micellar electrokinetic capillary chromatography".PHYTOCHEMICAL ANALYSIS 14.3(2003):132-136. |
入库方式： OAI收割
来源：化学研究所
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