Preparation approach of monolithic silica column
文献类型：期刊论文
| 作者 | Gao, WH; Yang, GL; Yang, J; Liu, HY; Yin, JF; Chen, Y |
| 刊名 | CHEMICAL JOURNAL OF CHINESE UNIVERSITIES-CHINESE
 |
| 出版日期 | 2004-12-10 |
| 卷号 | 25期号:12页码:2250-2252 |
| 关键词 | Monolithic Silica Column Sol-gel Technology High Performance Liquid Chromatography Pore Structure |
| ISSN号 | 0251-0790 |
| 英文摘要 | A new approach of preparing monolithic silica column was founded by adopting an improved solgel technology with tetramethoxysilane and polyethylene glycol as the matrix materials. The reason of resulting in crack and deformation of monolithic column was explained. By using N,N-dimethylformamide and a heat treatment procedure, the problems of crack and deformation in preparing the column were solved and the drying time was shortened greatly. In addition, the methods of fabricating mesopore and the effects of porogen solvent of different concentrations on monolithic silica column were investigated. The results show that the column prepared possessed bimodal pores structures with micrometer-size co-continuous through-pores and silica skeletons which have nanometer-size mesopores, straight appearance, high porosity, good chemical and mechanical stability. The characteristics would favour the separation with a rapid speed and high efficiency for both small molecules and macromolecules. |
| 语种 | 英语 |
| WOS记录号 | WOS:000225904200015 |
| 出版者 | HIGHER EDUCATION PRESS |
| 源URL | [http://ir.iccas.ac.cn/handle/121111/82423]  |
| 专题 | 中国科学院化学研究所 |
| 通讯作者 | Yang, GL |
| 作者单位 | 1.Hebei Univ, Coll Chem & Environm Sci, Baoding 071002, Peoples R China 2.Hebei Univ Sci & Technol, Coll Biol Sci & Engn, Shijiazhuang 050018, Peoples R China 3.Chinese Acad Sci, Inst Chem, Ctr Mol Sci, Beijing 100080, Peoples R China |
| 推荐引用方式 GB/T 7714 | Gao, WH,Yang, GL,Yang, J,et al. Preparation approach of monolithic silica column[J]. CHEMICAL JOURNAL OF CHINESE UNIVERSITIES-CHINESE,2004,25(12):2250-2252. |
| APA | Gao, WH,Yang, GL,Yang, J,Liu, HY,Yin, JF,&Chen, Y.(2004).Preparation approach of monolithic silica column.CHEMICAL JOURNAL OF CHINESE UNIVERSITIES-CHINESE,25(12),2250-2252. |
| MLA | Gao, WH,et al."Preparation approach of monolithic silica column".CHEMICAL JOURNAL OF CHINESE UNIVERSITIES-CHINESE 25.12(2004):2250-2252. |
入库方式： OAI收割
来源：化学研究所
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