A high-pressure single-crystal-diffraction experimental system at 4W2 beamline of BSRF
文献类型:期刊论文
作者 | Cui, WR![]() ![]() ![]() ![]() ![]() ![]() ![]() ![]() ![]() |
刊名 | JOURNAL OF SYNCHROTRON RADIATION
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出版日期 | 2017 |
卷号 | 24页码:699-706 |
关键词 | high pressure single crystal XRD |
ISSN号 | 1600-5775 |
DOI | 10.1107/S1600577517003393 |
文献子类 | Article |
英文摘要 | Information on the structural evolution of materials under high pressure is of great importance for understanding the properties of materials exhibited under high pressure. High-pressure powder diffraction is widely used to investigate the structure evolution of materials at such pressure. Unfortunately, powder diffraction data are usually insufficient for retrieving the atomic structures, with high-pressure single-crystal diffraction being more desirable for such a purpose. Here, a high-pressure single-crystal diffraction experimental system developed recently at beamline 4W2 of Beijing Synchrotron Radiation Facility (BSRF) is reported. The design and operation of this system are described with emphasis on special measures taken to allow for the special circumstance of high-pressure single-crystal diffraction. As an illustration, a series of diffraction datasets were collected on a single crystal of LaB6 using this system under various pressures (from ambient pressure to 39.1GPa). The quality of the datasets was found to be sufficient for structure solution and subsequent refinement. |
WOS关键词 | X-RAY-DIFFRACTION ; EXTREME CONDITIONS ; PHASE-TRANSITION ; PEROVSKITE ; CRYSTALLOGRAPHY ; ALGORITHM ; CELLS ; GPA |
WOS研究方向 | Instruments & Instrumentation ; Optics ; Physics |
语种 | 英语 |
WOS记录号 | WOS:000400385400020 |
源URL | [http://ir.ihep.ac.cn/handle/311005/284942] ![]() |
专题 | 高能物理研究所_多学科研究中心 |
作者单位 | 中国科学院高能物理研究所 |
推荐引用方式 GB/T 7714 | Cui, WR,Li XD,Li, XD,et al. A high-pressure single-crystal-diffraction experimental system at 4W2 beamline of BSRF[J]. JOURNAL OF SYNCHROTRON RADIATION,2017,24:699-706. |
APA | Cui, WR.,李晓东.,Li, XD.,李鹏善.,李蕊.,...&Li, YC.(2017).A high-pressure single-crystal-diffraction experimental system at 4W2 beamline of BSRF.JOURNAL OF SYNCHROTRON RADIATION,24,699-706. |
MLA | Cui, WR,et al."A high-pressure single-crystal-diffraction experimental system at 4W2 beamline of BSRF".JOURNAL OF SYNCHROTRON RADIATION 24(2017):699-706. |
入库方式: OAI收割
来源:高能物理研究所
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