Ultrasonic extraction and LC determination of linear alkylbenzene sulfonate in plant tissues
文献类型：期刊论文
| 作者 | Ou, ZQ; Jia, LQ; Jin, HY; Yediler, A; Sun, TH; Kettrup, A; Ou, ZQ, ACAD SINICA,INST APPL ECOL,OPEN LAB ECOL PROC TRACE SUBST TERR ECOSYST,SHENYANG 110015,PEOPLES R CHINA |
| 刊名 | CHROMATOGRAPHIA
 |
| 出版日期 | 1997 |
| 卷号 | 44期号:7-8页码:417-420 |
| 关键词 | Column Liquid Chromatography Plant Tissues Linear Alkylbenzene Sulfonate (Las) Rice |
| ISSN号 | 0009-5893 |
| 英文摘要 | A new method has been developed for the extraction and determination of linear alkylbenzene sulfonate (LAS) in plant tissues (rice stems and leaves). It consists of methanol-ultrasonic extraction followed by clean-up with aluminum oxide, enrichment with C-18 solid-phase extraction column and determination by HPLC. Both efficiency and accuracy of the overall method were high, i.e. mean recovery of: 89 % (84 to 93 % for LAS concentrations ranging from 1 to 100 mg kg(-1)) and repeatability of: 3 % relative standard deviation for 6 replicate analyses. With a 2 g sample for analysis, LAS levels of 0.5 mg kg(-1) in plants could be detected with the proposed method. Further advantages were: it was less time consuming (1 h for extraction), less solvent consumption, and smaller samples (2 to 3 g) required when compared with Soxhlet extraction. |
| 学科主题 | Biochemical Research Methods ; Chemistry, Analytical |
| 语种 | 英语 |
| 公开日期 | 2011-09-23 |
| 源URL | [http://210.72.129.5/handle/321005/55671]  |
| 专题 | 沈阳应用生态研究所_沈阳应用生态研究所 |
| 通讯作者 | Ou, ZQ, ACAD SINICA,INST APPL ECOL,OPEN LAB ECOL PROC TRACE SUBST TERR ECOSYST,SHENYANG 110015,PEOPLES R CHINA |
| 推荐引用方式 GB/T 7714 | Ou, ZQ,Jia, LQ,Jin, HY,et al. Ultrasonic extraction and LC determination of linear alkylbenzene sulfonate in plant tissues[J]. CHROMATOGRAPHIA,1997,44(7-8):417-420. |
| APA | Ou, ZQ.,Jia, LQ.,Jin, HY.,Yediler, A.,Sun, TH.,...&Ou, ZQ, ACAD SINICA,INST APPL ECOL,OPEN LAB ECOL PROC TRACE SUBST TERR ECOSYST,SHENYANG 110015,PEOPLES R CHINA.(1997).Ultrasonic extraction and LC determination of linear alkylbenzene sulfonate in plant tissues.CHROMATOGRAPHIA,44(7-8),417-420. |
| MLA | Ou, ZQ,et al."Ultrasonic extraction and LC determination of linear alkylbenzene sulfonate in plant tissues".CHROMATOGRAPHIA 44.7-8(1997):417-420. |
入库方式： OAI收割
来源：沈阳应用生态研究所
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