中国科学院机构知识库网格
Chinese Academy of Sciences Institutional Repositories Grid
Crystal and Molecular Structure of (S)-N-(2-Hydroxyphenyl)pyrrolidine-2-carboxamide

文献类型:期刊论文

作者Chen, Gang1; Tang, Ying1; Zhang, Qun-Zheng1; Meng, Mei1; Hao, Xiao-Jiang2
刊名JOURNAL OF CHEMICAL CRYSTALLOGRAPHY
出版日期2011-02-01
卷号41期号:2页码:251-254
关键词L-Proline (S)-N-(2-Hydroxyphenyl) pyrrolidine-2-carboxamide X-ray structure
ISSN号1074-1542
通讯作者Chen, G (reprint author), Xian Shiyou Univ, Coll Chem & Chem Engn, Xian 710065, Shaanxi, Peoples R China
英文摘要(S)-N-(2-Hydroxyphenyl)pyrrolidine-2-carboxamide was synthesized from Cbz-l-proline through two steps and characterized by NMR and MS. The crystal structure was determined from single-crystal X-ray diffraction data. It crystallizes in the monoclinic space group, P2(1), with unit cell dimensions a = 7.284(6) angstrom, b = 10.262(9) angstrom, and c = 7.975(7) angstrom, alpha = 90.00 degrees, beta = 114.451(14)degrees, gamma = 90.00 degrees and Z = 2. The absolute configuration of the chiral center is determined as S. In the crystal structure, intermolecular and intramolecular hydrogen bonds are responsible for the formation of a 1-dimensional network.
学科主题Crystallography; Spectroscopy
类目[WOS]Crystallography ; Spectroscopy
研究领域[WOS]Crystallography ; Spectroscopy
关键词[WOS]ASYMMETRIC ALDOL REACTIONS ; ORGANOCATALYSTS ; DESIGN ; ACID
收录类别SCI
资助信息Shaanxi Science and Technology Department[SJ08B20]; Shaanxi Education Department[09JK702]
语种英语
WOS记录号WOS:000286469800030
公开日期2012-04-10
源URL[http://ir.kib.ac.cn/handle/151853/5355]  
专题昆明植物研究所_植物化学与西部植物资源持续利用国家重点实验室
作者单位1.Xian Shiyou Univ, Coll Chem & Chem Engn, Xian 710065, Shaanxi, Peoples R China
2.Chinese Acad Sci, State Key Lab Phytochem & Plant Resources W China, Kunming Inst Bot, Kunming 650204, Yunnan, Peoples R China
推荐引用方式
GB/T 7714
Chen, Gang,Tang, Ying,Zhang, Qun-Zheng,et al. Crystal and Molecular Structure of (S)-N-(2-Hydroxyphenyl)pyrrolidine-2-carboxamide[J]. JOURNAL OF CHEMICAL CRYSTALLOGRAPHY,2011,41(2):251-254.
APA Chen, Gang,Tang, Ying,Zhang, Qun-Zheng,Meng, Mei,&Hao, Xiao-Jiang.(2011).Crystal and Molecular Structure of (S)-N-(2-Hydroxyphenyl)pyrrolidine-2-carboxamide.JOURNAL OF CHEMICAL CRYSTALLOGRAPHY,41(2),251-254.
MLA Chen, Gang,et al."Crystal and Molecular Structure of (S)-N-(2-Hydroxyphenyl)pyrrolidine-2-carboxamide".JOURNAL OF CHEMICAL CRYSTALLOGRAPHY 41.2(2011):251-254.

入库方式: OAI收割

来源:昆明植物研究所

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