Crystal and Molecular Structure of (S)-N-(2-Hydroxyphenyl)pyrrolidine-2-carboxamide
文献类型：期刊论文
| 作者 | Chen, Gang1; Tang, Ying1; Zhang, Qun-Zheng1; Meng, Mei1; Hao, Xiao-Jiang2
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| 刊名 | JOURNAL OF CHEMICAL CRYSTALLOGRAPHY
 |
| 出版日期 | 2011-02-01 |
| 卷号 | 41期号:2页码:251-254 |
| 关键词 | L-Proline (S)-N-(2-Hydroxyphenyl) pyrrolidine-2-carboxamide X-ray structure |
| ISSN号 | 1074-1542 |
| 通讯作者 | Chen, G (reprint author), Xian Shiyou Univ, Coll Chem & Chem Engn, Xian 710065, Shaanxi, Peoples R China |
| 英文摘要 | (S)-N-(2-Hydroxyphenyl)pyrrolidine-2-carboxamide was synthesized from Cbz-l-proline through two steps and characterized by NMR and MS. The crystal structure was determined from single-crystal X-ray diffraction data. It crystallizes in the monoclinic space group, P2(1), with unit cell dimensions a = 7.284(6) angstrom, b = 10.262(9) angstrom, and c = 7.975(7) angstrom, alpha = 90.00 degrees, beta = 114.451(14)degrees, gamma = 90.00 degrees and Z = 2. The absolute configuration of the chiral center is determined as S. In the crystal structure, intermolecular and intramolecular hydrogen bonds are responsible for the formation of a 1-dimensional network. |
| 学科主题 | Crystallography; Spectroscopy |
| 类目[WOS] | Crystallography ; Spectroscopy |
| 研究领域[WOS] | Crystallography ; Spectroscopy |
| 关键词[WOS] | ASYMMETRIC ALDOL REACTIONS ; ORGANOCATALYSTS ; DESIGN ; ACID |
| 收录类别 | SCI |
| 资助信息 | Shaanxi Science and Technology Department[SJ08B20]; Shaanxi Education Department[09JK702] |
| 语种 | 英语 |
| WOS记录号 | WOS:000286469800030 |
| 公开日期 | 2012-04-10 |
| 源URL | [http://ir.kib.ac.cn/handle/151853/5355]  |
| 专题 | 昆明植物研究所_植物化学与西部植物资源持续利用国家重点实验室 |
| 作者单位 | 1.Xian Shiyou Univ, Coll Chem & Chem Engn, Xian 710065, Shaanxi, Peoples R China 2.Chinese Acad Sci, State Key Lab Phytochem & Plant Resources W China, Kunming Inst Bot, Kunming 650204, Yunnan, Peoples R China |
| 推荐引用方式 GB/T 7714 | Chen, Gang,Tang, Ying,Zhang, Qun-Zheng,et al. Crystal and Molecular Structure of (S)-N-(2-Hydroxyphenyl)pyrrolidine-2-carboxamide[J]. JOURNAL OF CHEMICAL CRYSTALLOGRAPHY,2011,41(2):251-254. |
| APA | Chen, Gang,Tang, Ying,Zhang, Qun-Zheng,Meng, Mei,&Hao, Xiao-Jiang.(2011).Crystal and Molecular Structure of (S)-N-(2-Hydroxyphenyl)pyrrolidine-2-carboxamide.JOURNAL OF CHEMICAL CRYSTALLOGRAPHY,41(2),251-254. |
| MLA | Chen, Gang,et al."Crystal and Molecular Structure of (S)-N-(2-Hydroxyphenyl)pyrrolidine-2-carboxamide".JOURNAL OF CHEMICAL CRYSTALLOGRAPHY 41.2(2011):251-254. |
入库方式： OAI收割
来源：昆明植物研究所
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