In-situ energy calibration of SSRF macromolecular crystallography beamline using powder diffraction
文献类型：期刊论文
| 作者 | Tao Shixing(陶世兴) ; Zhu Jing(朱静) ; Niu Jing ; Chen Mingzhi(陈鸣之) ; Liu Ke（刘科） ; Wang Yu（王玉） ; Wang Qisheng（汪启胜） ; Sun Bo（孙波） ; Huang Sheng(黄胜) ; Tang Lin(唐琳) ; He Jianhua(何建华) |
| 刊名 | NUCLEAR SCIENCE AND TECHNIQUES
 |
| 出版日期 | 2010 |
| 卷号 | 21期号:6页码:4 |
| 关键词 | X-ray Energy calibration Powder diffraction Beamline |
| ISSN号 | 1001-8042 |
| 通讯作者 | He, JH (reprint author), Chinese Acad Sci, Shanghai Inst Appl Phys, Shanghai 201800, Peoples R China |
| 英文摘要 | For X-ray powder diffraction spectra collected by an area detector of MarCCD on macromolecular crystallography beamline of SSRF, an energy calibration method was developed using LaB(6)(660a) powder diffraction for in-situ rapid energy calibration of the X-rays without changing the experimental conditions. The intensity of each diffraction ring was integrated, and the accurate peak positions were fitted by Pseudo-Voigt function model. The sample's interplanar spacing for XRD analysis and the calibrated energy were obtained by the PCPDFWIN code and by fitting all the energies with the least-square method. The exposure time and the sample to-detector distance were found no effect on accuracy of the energy calibration, and the in-situ energy calibration could be done with an accuracy of better than 0.4 parts per thousand in 7-18 keV. This method is applicable to other X-ray beamlines. |
| 学科主题 | Nuclear Science & Technology; Physics |
| 收录类别 | SCI |
| 语种 | 英语 |
| WOS记录号 | WOS:000287642700001 |
| 公开日期 | 2012-04-11 |
| 源URL | [http://ir.sinap.ac.cn/handle/331007/6943]  |
| 专题 | 上海应用物理研究所_中科院上海应用物理研究所2004-2010年 |
| 推荐引用方式 GB/T 7714 | Tao Shixing,Zhu Jing,Niu Jing,et al. In-situ energy calibration of SSRF macromolecular crystallography beamline using powder diffraction[J]. NUCLEAR SCIENCE AND TECHNIQUES,2010,21(6):4. |
| APA | Tao Shixing.,Zhu Jing.,Niu Jing.,Chen Mingzhi.,Liu Ke.,...&He Jianhua.(2010).In-situ energy calibration of SSRF macromolecular crystallography beamline using powder diffraction.NUCLEAR SCIENCE AND TECHNIQUES,21(6),4. |
| MLA | Tao Shixing,et al."In-situ energy calibration of SSRF macromolecular crystallography beamline using powder diffraction".NUCLEAR SCIENCE AND TECHNIQUES 21.6(2010):4. |
入库方式： OAI收割
来源：上海应用物理研究所
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