Poly(methacrylic acid-co-ethylene glycol dimethacrylate) monolith microextraction coupled with high performance liquid chromatography for the determination of phthalate esters in cosmetics
文献类型：期刊论文
| 作者 | Su RY ; Zhao XW ; Li ZY ; Jia QO ; Liu P ; Jia JB |
| 刊名 | analytica chimica acta
 |
| 出版日期 | 2010 |
| 卷号 | 676期号:1-2页码:103-108 |
| 关键词 | SOLID-PHASE EXTRACTION ENVIRONMENTAL WATER SAMPLES FLUORESCENCE DETECTION NITRIC-OXIDE SENSITIVE DETERMINATION HPLC-UV CAPILLARY DERIVATIZATION ENRICHMENT NANOTUBES |
| ISSN号 | 0003-2670 |
| 通讯作者 | jia qo |
| 中文摘要 | a simple, sensitive, and rapid strategy has been reported in this work which is based on polymer monolith microextraction (pmme) and high performance liquid chromatography (hplc) for the determination of phthalate esters in cosmetics. a poly(methacrylic acid-co-ethylene glycol dimethacrylate)(maa-egdma) monolithic capillary column is selected as the extraction medium for pmme. in order to obtain optimum extraction efficiency, the conditions of pmme including sample flow rate, sample volume, sample ph, and eluent flow rate have been investigated. under the optimum conditions, the limits of detection for dimethyl phthalate (dmp), di-n-butyl phthalate (dbp), dicyclohexyl phthalate (dchp), and di-n-octyl phthalate (dop) based three times of standard deviations of blank by seven replicated are in the range of 0.7-3.7 ng ml(-1). the reproducibility of the method is obtained with intra-day and inter-day relative standard deviations less than 3.2% and 7.7%, respectively. the method has been successfully applied to the determination of the four phthalate esters in cosmetics with a recovery range of 81.2-108.8% in all the samples. (c) 2010 elsevier b.v. all rights reserved. |
| 收录类别 | SCI收录期刊论文 |
| 语种 | 英语 |
| WOS记录号 | WOS:000281990500015 |
| 公开日期 | 2012-04-26 |
| 源URL | [http://ir.ciac.jl.cn/handle/322003/43469]  |
| 专题 | 长春应用化学研究所_长春应用化学研究所知识产出_期刊论文 |
| 推荐引用方式 GB/T 7714 | Su RY,Zhao XW,Li ZY,et al. Poly(methacrylic acid-co-ethylene glycol dimethacrylate) monolith microextraction coupled with high performance liquid chromatography for the determination of phthalate esters in cosmetics[J]. analytica chimica acta,2010,676(1-2):103-108. |
| APA | Su RY,Zhao XW,Li ZY,Jia QO,Liu P,&Jia JB.(2010).Poly(methacrylic acid-co-ethylene glycol dimethacrylate) monolith microextraction coupled with high performance liquid chromatography for the determination of phthalate esters in cosmetics.analytica chimica acta,676(1-2),103-108. |
| MLA | Su RY,et al."Poly(methacrylic acid-co-ethylene glycol dimethacrylate) monolith microextraction coupled with high performance liquid chromatography for the determination of phthalate esters in cosmetics".analytica chimica acta 676.1-2(2010):103-108. |
入库方式： OAI收割
来源：长春应用化学研究所
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