Preparation of highly dispersed antimony-doped tin oxide nanopowders by azeotropie drying with isoamyl acetate
文献类型：期刊论文
| 作者 | Y. Fen ; X. Zhang ; W. Xu ; T. Fang ; F. Gan |
| 刊名 | Transactions of Nonferrous Metals Society of China
 |
| 出版日期 | 2007 |
| 卷号 | 17期号:3页码:626-632 |
| 关键词 | antimony-doped tin oxide nanopowder dispersivity azeotropic drying isoamylacetate powders nanoparticles |
| ISSN号 | 1003-6326 |
| 中文摘要 | Antimony-doped tin hydroxide colloid precipitates were prepared by hydrolysis of SnCl4 center dot 5H(2)O and SbCl3 ethanol solutions. Isoamyl acetate was selected as azeotropic drying solvent and was compared with the most commonly used n-butanol solvent on treating precipitate for low hard agglomeration precursor powders. The FT-IR, BET, XRD, and TEM results of the precursor powders and calcinated antimony-doped tin oxide powders were recorded. The results demonstrate that isoamyl acetate is an excellent azeotropic drying solvent that can effectively prevent the agglomeration of particles and greatly improve the fluffiness of the obtained dried powders. After these precursor powders are calcined, antimony-doped tin oxide nanopowders with tetragonal rutile structure and high dispersivity can be obtained. |
| 原文出处 | |
| 公开日期 | 2012-04-13 |
| 源URL | [http://ir.imr.ac.cn/handle/321006/33527]  |
| 专题 | 金属研究所_中国科学院金属研究所 |
| 推荐引用方式 GB/T 7714 | Y. Fen,X. Zhang,W. Xu,et al. Preparation of highly dispersed antimony-doped tin oxide nanopowders by azeotropie drying with isoamyl acetate[J]. Transactions of Nonferrous Metals Society of China,2007,17(3):626-632. |
| APA | Y. Fen,X. Zhang,W. Xu,T. Fang,&F. Gan.(2007).Preparation of highly dispersed antimony-doped tin oxide nanopowders by azeotropie drying with isoamyl acetate.Transactions of Nonferrous Metals Society of China,17(3),626-632. |
| MLA | Y. Fen,et al."Preparation of highly dispersed antimony-doped tin oxide nanopowders by azeotropie drying with isoamyl acetate".Transactions of Nonferrous Metals Society of China 17.3(2007):626-632. |
入库方式： OAI收割
来源：金属研究所
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