Synthesis and TEM observation of fluffy hollow carbon spheres by FeCl(3) catalyzed solvent-thermal reaction
文献类型：期刊论文
| 作者 | C. L. Yin ; Q. H. Huang ; B. R. Liu ; X. F. Wang ; Y. G. Xie ; L. L. He ; M. Y. Zhang ; X. Yang |
| 刊名 | Materials Letters
 |
| 出版日期 | 2007 |
| 卷号 | 61期号:19-20页码:4015-4018 |
| 关键词 | hollow carbon spheres solvent-thermal reaction electron microscopy microstructure nanospheres route |
| ISSN号 | 0167-577X |
| 中文摘要 | Fluffy hollow carbon spheres with the diameter of 0.3-1.8 mu m and shell thickness of 30-80 nm were successfully synthesized via FeCl(3) catalyzed solvent-thermal reaction in a scaled autoclave at 350 degrees C for 3 h, with CaC(2) and CCl(4) as carbon sources and reactants. XRD and TEM observations verify that the fluffy hollow carbon spheres are composed of curved and disordered carbon flakes with the interlayer instance of approximate 0.35 nm. Furthermore, MCNTs with Fe-Mn-Cr nanorods encapsulated are also observed. A possible growth mechanism for the fluffy hollow carbon sphere is proposed. (c) 2007 Elsevier B.V. All rights reserved. |
| 原文出处 | |
| 公开日期 | 2012-04-13 |
| 源URL | [http://ir.imr.ac.cn/handle/321006/33994]  |
| 专题 | 金属研究所_中国科学院金属研究所 |
| 推荐引用方式 GB/T 7714 | C. L. Yin,Q. H. Huang,B. R. Liu,et al. Synthesis and TEM observation of fluffy hollow carbon spheres by FeCl(3) catalyzed solvent-thermal reaction[J]. Materials Letters,2007,61(19-20):4015-4018. |
| APA | C. L. Yin.,Q. H. Huang.,B. R. Liu.,X. F. Wang.,Y. G. Xie.,...&X. Yang.(2007).Synthesis and TEM observation of fluffy hollow carbon spheres by FeCl(3) catalyzed solvent-thermal reaction.Materials Letters,61(19-20),4015-4018. |
| MLA | C. L. Yin,et al."Synthesis and TEM observation of fluffy hollow carbon spheres by FeCl(3) catalyzed solvent-thermal reaction".Materials Letters 61.19-20(2007):4015-4018. |
入库方式： OAI收割
来源：金属研究所
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