Synthesis of 3,6-bisubstituted phenyl-bi-1,2,4-triazolo 3,4-b 1,3,4-thiadiazole derivatives
文献类型：期刊论文
| 作者 | J. H. Qian ; L. Liu ; D. L. Wang ; J. J. Xing |
| 刊名 | Chinese Journal of Organic Chemistry
 |
| 出版日期 | 2006 |
| 卷号 | 26期号:12页码:1720-1722 |
| 关键词 | POCl3 2 triazolo-1 5-bihydrazino-1 3 3 4-thiadiazole 4-thiadiazol mechanism |
| ISSN号 | 0253-2786 |
| 中文摘要 | 2,5-Bihydrazino-1,3,4-thiadiazole was synthesized by substitution of 2,5-bimercapto-1,3,4-thiadiazole with hydrazine hydrate and reacted with benzoyl chloride to give 2,5-biacylhydrazino-1,3,4-thiadiazole, which was further ring-closed by POCl3 as cyclization agent to synthesize 3,6-bisubstituted phenyl-bi-1,2,4-triazolo[3,4-b]-1,3,4-thiadiazole derivatives. The novel compounds were confirmed by elemental analysis, IR, H-1 NMR and MS spectra. The mechanism of cycloreaction was also discussed. |
| 原文出处 | |
| 公开日期 | 2012-04-14 |
| 源URL | [http://ir.imr.ac.cn/handle/321006/34427]  |
| 专题 | 金属研究所_中国科学院金属研究所 |
| 推荐引用方式 GB/T 7714 | J. H. Qian,L. Liu,D. L. Wang,et al. Synthesis of 3,6-bisubstituted phenyl-bi-1,2,4-triazolo 3,4-b 1,3,4-thiadiazole derivatives[J]. Chinese Journal of Organic Chemistry,2006,26(12):1720-1722. |
| APA | J. H. Qian,L. Liu,D. L. Wang,&J. J. Xing.(2006).Synthesis of 3,6-bisubstituted phenyl-bi-1,2,4-triazolo 3,4-b 1,3,4-thiadiazole derivatives.Chinese Journal of Organic Chemistry,26(12),1720-1722. |
| MLA | J. H. Qian,et al."Synthesis of 3,6-bisubstituted phenyl-bi-1,2,4-triazolo 3,4-b 1,3,4-thiadiazole derivatives".Chinese Journal of Organic Chemistry 26.12(2006):1720-1722. |
入库方式： OAI收割
来源：金属研究所
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