Preparation of single-crystal alpha-MnO2 nanorods and nanoneedles from aqueous solution
文献类型:期刊论文
作者 | Y. Chen ; C. Liu ; F. Li ; H. M. Cheng |
刊名 | Journal of Alloys and Compounds
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出版日期 | 2005 |
卷号 | 397期号:1-2页码:282-285 |
关键词 | X-ray diffraction nanostructures scanning and transmission electron microscopy open tunnel mno2 nanowires batteries electrode zinc |
ISSN号 | 0925-8388 |
中文摘要 | Single-crystal alpha-MnO2 nanorods and nanoneedles were prepared in H2SO4 solution by adding KMnO4 at temperature of 70-95 degrees C. The morphologies of the as-synthesized products were examined by scanning electron microscopy (SEM) and transmission electron microscopy (TEM) and high-resolution transmission electron microscopy. X-ray diffraction (XRD), energy dispersive spectroscopy (EDS), and cryonitrogen adsorption measurements were also employed for characterization of the nanostructures. The results show that pure alpha-MnO2, nanorods with diameters of 12-20 nm and nanoneedles with diameters of 5-8 nm were synthesized by this technique. A high specific surface area of 165.8 m(2)/g was achieved for the alpha-MnO2 nanoneedles with a small diameter of 5 nm. (c) 2005 Elsevier B.V. All rights reserved. |
原文出处 | |
公开日期 | 2012-04-14 |
源URL | [http://ir.imr.ac.cn/handle/321006/34819] ![]() |
专题 | 金属研究所_中国科学院金属研究所 |
推荐引用方式 GB/T 7714 | Y. Chen,C. Liu,F. Li,et al. Preparation of single-crystal alpha-MnO2 nanorods and nanoneedles from aqueous solution[J]. Journal of Alloys and Compounds,2005,397(1-2):282-285. |
APA | Y. Chen,C. Liu,F. Li,&H. M. Cheng.(2005).Preparation of single-crystal alpha-MnO2 nanorods and nanoneedles from aqueous solution.Journal of Alloys and Compounds,397(1-2),282-285. |
MLA | Y. Chen,et al."Preparation of single-crystal alpha-MnO2 nanorods and nanoneedles from aqueous solution".Journal of Alloys and Compounds 397.1-2(2005):282-285. |
入库方式: OAI收割
来源:金属研究所
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