Intermediate phases in Ti3SiC2 synthesis from Ti/SiC/C mixtures studied by time-resolved neutron diffraction
文献类型:期刊论文
作者 | E. D. Wu ; E. H. Kisi ; D. P. Riley ; R. I. Smith |
刊名 | Journal of the American Ceramic Society
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出版日期 | 2002 |
卷号 | 85期号:12页码:3084-3086 |
关键词 | powder diffraction |
ISSN号 | 0002-7820 |
中文摘要 | The reactive sintering of 3Ti/SiC/C to form the layered ternary carbide Ti3SiC2 was studied in situ by time-resolved neutron powder diffraction. A number of intermediate processes occur during the synthesis beginning with the alpha-beta transition in Ti. Concurrent with the alpha-beta transition, two intermediate phases, TiCx and Ti5Si3Cx (x less than or equal to 1), form. These phases account for almost the entire sample in the range 1500-1600degreesC beyond which they react with each other and a small amount of free C to form the product phase Ti3SiC2. |
原文出处 | |
公开日期 | 2012-04-14 |
源URL | [http://ir.imr.ac.cn/handle/321006/36452] ![]() |
专题 | 金属研究所_中国科学院金属研究所 |
推荐引用方式 GB/T 7714 | E. D. Wu,E. H. Kisi,D. P. Riley,et al. Intermediate phases in Ti3SiC2 synthesis from Ti/SiC/C mixtures studied by time-resolved neutron diffraction[J]. Journal of the American Ceramic Society,2002,85(12):3084-3086. |
APA | E. D. Wu,E. H. Kisi,D. P. Riley,&R. I. Smith.(2002).Intermediate phases in Ti3SiC2 synthesis from Ti/SiC/C mixtures studied by time-resolved neutron diffraction.Journal of the American Ceramic Society,85(12),3084-3086. |
MLA | E. D. Wu,et al."Intermediate phases in Ti3SiC2 synthesis from Ti/SiC/C mixtures studied by time-resolved neutron diffraction".Journal of the American Ceramic Society 85.12(2002):3084-3086. |
入库方式: OAI收割
来源:金属研究所
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