HREM observations of the synthesized process of nano-sized SiC by ball milling of Si and C mixed powders
文献类型:期刊论文
作者 | X. Y. Yang ; Z. W. Huang ; Y. K. Wu ; H. Q. Ye |
刊名 | Materials Science and Engineering a-Structural Materials Properties Microstructure and Processing
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出版日期 | 2001 |
卷号 | 300期号:1-2页码:278-283 |
关键词 | Si-C system ball milling high-resolution electronic microscopy elemental powders temperature silicon mechanosynthesis transition |
ISSN号 | 0921-5093 |
中文摘要 | The synthesis of nano-sized SiC through ball milling (BM) of elemental Si and graphite mixed powders at room temperature has been reported, and detailed reaction process has been characterized by high-resolution electron microscopy (HREM). High-resolution electron microscopy (HREM) observations presented herein suggest that amorphous graphite (a-graphite), amorphous silicon (a-Si) and nano-sized crystalline Si (c-Si) with many defects are produced during BM, which is prerequisite to the reaction. In some areas, SIC is synthesized through a diffusion of C atoms into the a-Si/and c-Si. In the former, a-Si(C) forms, and then mechanically-driven crystallization of the a-Si(C) occurs to form SIG. In the latter, C atoms directly replace Si atoms to form SIC with an orientation relationship of (111)(SiC)//(111)(Si). In other areas, localized self-sustained reaction occurs to form slightly larger SIC grains. (C) 2001 Elsevier Science B.V. All rights reserved. |
原文出处 | |
公开日期 | 2012-04-14 |
源URL | [http://ir.imr.ac.cn/handle/321006/36869] ![]() |
专题 | 金属研究所_中国科学院金属研究所 |
推荐引用方式 GB/T 7714 | X. Y. Yang,Z. W. Huang,Y. K. Wu,et al. HREM observations of the synthesized process of nano-sized SiC by ball milling of Si and C mixed powders[J]. Materials Science and Engineering a-Structural Materials Properties Microstructure and Processing,2001,300(1-2):278-283. |
APA | X. Y. Yang,Z. W. Huang,Y. K. Wu,&H. Q. Ye.(2001).HREM observations of the synthesized process of nano-sized SiC by ball milling of Si and C mixed powders.Materials Science and Engineering a-Structural Materials Properties Microstructure and Processing,300(1-2),278-283. |
MLA | X. Y. Yang,et al."HREM observations of the synthesized process of nano-sized SiC by ball milling of Si and C mixed powders".Materials Science and Engineering a-Structural Materials Properties Microstructure and Processing 300.1-2(2001):278-283. |
入库方式: OAI收割
来源:金属研究所
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