Synthesis and characterization of rutile TiO2 nanowhiskers
文献类型:期刊论文
作者 | G. L. Li ; G. H. Wang ; J. M. Hong |
刊名 | Journal of Materials Research
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出版日期 | 1999 |
卷号 | 14期号:8页码:3346-3354 |
关键词 | titania microemulsions growth powders surface coprecipitation transformation temperature precursors nanowires |
ISSN号 | 0884-2914 |
中文摘要 | Rutile TiO2, nanowhiskers have been synthesized by annealing a precursor powder in which NaCl and Ti(OH), particles were homogeneously mixed. The precursor powder was prepared by mixing three kinds of inverse microemulsions (mu E) containing TiCl4, aqueous solution, ammonia, and NaCl aqueous solution, respectively, followed by washing with acetone. Annealing temperature and packing density of Ti(OH), in the precursor powder influenced the formation of rutile nanowhiskers. The optimum temperature was 750 degrees C. TiO2, nanowhiskers obtained by annealing a precursor powder in which the molar ratio of sodium to titanium was 400 at 750 degrees C for 2 h had diameters of 10-50 nm and lengths of several micrometers. They were straight rods with square cross sections, and the side surfaces were composed of four equivalent (110) planes. |
原文出处 | |
公开日期 | 2012-04-14 |
源URL | [http://ir.imr.ac.cn/handle/321006/37397] ![]() |
专题 | 金属研究所_中国科学院金属研究所 |
推荐引用方式 GB/T 7714 | G. L. Li,G. H. Wang,J. M. Hong. Synthesis and characterization of rutile TiO2 nanowhiskers[J]. Journal of Materials Research,1999,14(8):3346-3354. |
APA | G. L. Li,G. H. Wang,&J. M. Hong.(1999).Synthesis and characterization of rutile TiO2 nanowhiskers.Journal of Materials Research,14(8),3346-3354. |
MLA | G. L. Li,et al."Synthesis and characterization of rutile TiO2 nanowhiskers".Journal of Materials Research 14.8(1999):3346-3354. |
入库方式: OAI收割
来源:金属研究所
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