Polymorphic Transformation of Isotactic Poly(1-butene) in Form III upon Heating: In Situ Synchrotron Small- and Wide-Angle X-ray Scattering Studies
文献类型：期刊论文
| 作者 | Jiang ZY ; Sun YY ; Tang YJ ; Lai YQ ; Funari SS ; Gehrke R ; Men YF |
| 刊名 | journal of physical chemistry b
 |
| 出版日期 | 2010 |
| 卷号 | 114期号:18页码:6001-6005 |
| ISSN号 | 1520-6106 |
| 关键词 | CRYSTAL-CRYSTAL TRANSFORMATIONS POLYBUTENE-1 SINGLE-CRYSTALS C-13 NMR-SPECTROSCOPY PHASE-TRANSFORMATION EPITAXIAL CRYSTALLIZATION MICROINDENTATION HARDNESS DEFORMATION MORPHOLOGY POLY-1-BUTENE TRANSITION |
| 通讯作者 | men yf |
| 中文摘要 | the phase transformation of form iii isotactic poly(1-butene) was investigated as a function of temperature. the polymer was isothermally precipitated from a dilute solution in iso-amyl acetate and observed with real-time synchrotron small- and wide-angle x-ray scattering techniques. the results confirmed that the polymorphic transition of form iii was strongly dependent on temperature. the phase transformation from form iii to form i' proceeded at a temperature of ca. 80 degrees c. this was accompanied by the presence of two distinctly different lamellar periodicities arising from form iii and i' crystals, respectively. the coexistence of form iii and i' crystals can persist up to 103 degrees c, followed by melting and recrystallizing into form ii crystals. finally, the reflections resulting from form ii crystals disappeared at 118 degrees c. |
| 收录类别 | SCI收录期刊论文 |
| 语种 | 英语 |
| WOS记录号 | WOS:000277280500005 |
| 公开日期 | 2012-06-06 |
| 源URL | [http://ir.ciac.jl.cn/handle/322003/43741]  |
| 专题 | 长春应用化学研究所_长春应用化学研究所知识产出_期刊论文 |
| 推荐引用方式 GB/T 7714 | Jiang ZY,Sun YY,Tang YJ,et al. Polymorphic Transformation of Isotactic Poly(1-butene) in Form III upon Heating: In Situ Synchrotron Small- and Wide-Angle X-ray Scattering Studies[J]. journal of physical chemistry b,2010,114(18):6001-6005. |
| APA | Jiang ZY.,Sun YY.,Tang YJ.,Lai YQ.,Funari SS.,...&Men YF.(2010).Polymorphic Transformation of Isotactic Poly(1-butene) in Form III upon Heating: In Situ Synchrotron Small- and Wide-Angle X-ray Scattering Studies.journal of physical chemistry b,114(18),6001-6005. |
| MLA | Jiang ZY,et al."Polymorphic Transformation of Isotactic Poly(1-butene) in Form III upon Heating: In Situ Synchrotron Small- and Wide-Angle X-ray Scattering Studies".journal of physical chemistry b 114.18(2010):6001-6005. |
入库方式： OAI收割
来源：长春应用化学研究所
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