Comparison of headspace solid-phase microextraction with conventional extraction for the analysis of the volatile components in Melia azedarach
文献类型：期刊论文
| 作者 | Yang YQ ; Xiao YM ; Liu BF ; Fang XX ; Yang W ; Xu JW |
| 刊名 | talanta
 |
| 出版日期 | 2011 |
| 卷号 | 86页码:356-361 |
| 关键词 | CHROMATOGRAPHY-MASS-SPECTROMETRY GAS-CHROMATOGRAPHY CYTOTOXIC ACTIVITY GC-MS ANTIFEEDANT ACTIVITY ESSENTIAL OILS LIMONOIDS TOOSENDAN FRUIT IDENTIFICATION |
| ISSN号 | 0039-9140 |
| 通讯作者 | yang w |
| 中文摘要 | the volatile compositions of melia azedarach were studied by headspace solid-phase microextraction (hs-spme). the result was compared with that obtained by soxhlet extraction (se) and ultrasonic extraction (uae). 79 compounds were identified in this study, among which 64 compounds were first reported. the experimental parameters including fiber type (pdms, pdms-dvb and car-pdms), desorption time, extraction temperature and time were investigated. 37 compounds were obtained by hs-spme, including curcumene (33.25%), alpha-cadinol (11.16%), alpha-muurolene (8.72%), copaene (5.04%), beta-bisabolene (3.41%), and a-selinene (2.97%). the result suggested that the hs-spme method is a powerful analytic tool and complementary to traditional methods for the determination of the volatile compounds in chinese herbs. (c) 2011 elsevier b.v. all rights reserved. |
| 收录类别 | SCI收录期刊论文 |
| 语种 | 英语 |
| WOS记录号 | WOS:000298126300046 |
| 公开日期 | 2012-06-08 |
| 源URL | [http://ir.ciac.jl.cn/handle/322003/44269]  |
| 专题 | 长春应用化学研究所_长春应用化学研究所知识产出_期刊论文 |
| 推荐引用方式 GB/T 7714 | Yang YQ,Xiao YM,Liu BF,et al. Comparison of headspace solid-phase microextraction with conventional extraction for the analysis of the volatile components in Melia azedarach[J]. talanta,2011,86:356-361. |
| APA | Yang YQ,Xiao YM,Liu BF,Fang XX,Yang W,&Xu JW.(2011).Comparison of headspace solid-phase microextraction with conventional extraction for the analysis of the volatile components in Melia azedarach.talanta,86,356-361. |
| MLA | Yang YQ,et al."Comparison of headspace solid-phase microextraction with conventional extraction for the analysis of the volatile components in Melia azedarach".talanta 86(2011):356-361. |
入库方式： OAI收割
来源：长春应用化学研究所
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