Application of poly(butyl methacrylate-co-ethylene glycol dimethacrylate) monolith microextraction coupled with high performance liquid chromatography to the determination of polycyclic aromatic hydrocarbons in smoked meat products
文献类型:期刊论文
作者 | Liu W ; Qi JR ; Yan LN ; Jia Q ; Yu C |
刊名 | journal of chromatography b-analytical technologies in the biomedical and life sciences
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出版日期 | 2011 |
卷号 | 879期号:28页码:3012-3016 |
关键词 | SOLID-PHASE MICROEXTRACTION CAPILLARY-ZONE-ELECTROPHORESIS MICROWAVE-ASSISTED EXTRACTION CLOUD-POINT EXTRACTION MASS-SPECTROMETRY FLUORESCENCE DETECTION SOLVENT-EXTRACTION GOLD NANOPARTICLES WATER SAMPLES COLUMN |
ISSN号 | 1570-0232 |
通讯作者 | jia q |
中文摘要 | this paper presents a study of the synthesis of a polymer monolith column and its application to the analysis of pahs in smoked meat products. a poly(butyl methacrylate-co-ethylene glycol dimethacrylate) monolith capillary has been successfully prepared with in situ polymerization method. the polymer monolith microextraction combined with hplc determinations is employed for the analysis of naphthalene, biphenyl, phenanthrene, and anthracene. various parameters affecting the extraction efficiency have been investigated and optimized. under the optimum experimental conditions, the method provides an acceptable linearity (2-10,000 mu g/l), low limits of detection (1.4-2.0 mu g/l), and good precision (intraday relative standard deviations < 4.1%, interday relative standard deviations < 5.7%). when applied to the determination of the four pahs in smoked meat samples, recoveries are obtained in the range of 86.6-101.5%. (c) 2011 elsevier b.v. all rights reserved. |
收录类别 | SCI收录期刊论文 |
语种 | 英语 |
WOS记录号 | WOS:000296073800011 |
公开日期 | 2012-06-08 |
源URL | [http://ir.ciac.jl.cn/handle/322003/44280] ![]() |
专题 | 长春应用化学研究所_长春应用化学研究所知识产出_期刊论文 |
推荐引用方式 GB/T 7714 | Liu W,Qi JR,Yan LN,et al. Application of poly(butyl methacrylate-co-ethylene glycol dimethacrylate) monolith microextraction coupled with high performance liquid chromatography to the determination of polycyclic aromatic hydrocarbons in smoked meat products[J]. journal of chromatography b-analytical technologies in the biomedical and life sciences,2011,879(28):3012-3016. |
APA | Liu W,Qi JR,Yan LN,Jia Q,&Yu C.(2011).Application of poly(butyl methacrylate-co-ethylene glycol dimethacrylate) monolith microextraction coupled with high performance liquid chromatography to the determination of polycyclic aromatic hydrocarbons in smoked meat products.journal of chromatography b-analytical technologies in the biomedical and life sciences,879(28),3012-3016. |
MLA | Liu W,et al."Application of poly(butyl methacrylate-co-ethylene glycol dimethacrylate) monolith microextraction coupled with high performance liquid chromatography to the determination of polycyclic aromatic hydrocarbons in smoked meat products".journal of chromatography b-analytical technologies in the biomedical and life sciences 879.28(2011):3012-3016. |
入库方式: OAI收割
来源:长春应用化学研究所
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