Determination of nitroanilines in hair dye using polymer monolith microextraction coupled with HPLC
文献类型：期刊论文
| 作者 | Xiao PF ; Bao CL ; Jia QO ; Su RY ; Zhou WH ; Jia JB |
| 刊名 | journal of separation science
 |
| 出版日期 | 2011 |
| 卷号 | 34期号:6页码:675-680 |
| 关键词 | SOLID-PHASE MICROEXTRACTION PERFORMANCE LIQUID-CHROMATOGRAPHY CAPILLARY-ZONE-ELECTROPHORESIS ENVIRONMENTAL WATER SAMPLES AROMATIC-AMINES HOLLOW-FIBER GAS-CHROMATOGRAPHY MASS-SPECTROMETRY SINGLE-DROP SPECTROPHOTOMETRIC DETERMINATION |
| ISSN号 | 1615-9306 |
| 通讯作者 | jia qo |
| 中文摘要 | in this study, a novel method for the determination of nitroanilines in hair dye samples has been developed based on poly(methacrylic acid-co-ethylene glycol dimethacrylate) monolith microextraction (pmme) and high-performance liquid chromatography (hplc) analysis. four nitroanilines, p-nitroaniline (pnal), m-nitroaniline (mnal), o-nitroaniline (onal), and 2,4-dinitroaniline (dnal), are studied as representatives. to obtain optimum extraction efficiency, several experimental parameters including sample flow rate, sample volume, sample ph, and eluent flow rate have been investigated. under the optimal experimental conditions, the linear regression coefficients of the standard curves are greater than 0.9990. the limits of detection for p-nitroaniline, m-nitroaniline, o-nitroaniline, and 2,4-dinitroaniline are 0.012, 0.008, 0.018, and 0.005 mu g/ml, respectively. the intraday and interday relative standard deviations are less than 3.1 and 5.4%, respectively. the proposed method is simple, rapid, sensitive, and competent when used for the determination of nitroanilines in hair dye samples and the accuracy is assessed through recovery experiments. |
| 收录类别 | SCI收录期刊论文 |
| 语种 | 英语 |
| WOS记录号 | WOS:000288545300010 |
| 公开日期 | 2012-06-11 |
| 源URL | [http://ir.ciac.jl.cn/handle/322003/44789]  |
| 专题 | 长春应用化学研究所_长春应用化学研究所知识产出_期刊论文 |
| 推荐引用方式 GB/T 7714 | Xiao PF,Bao CL,Jia QO,et al. Determination of nitroanilines in hair dye using polymer monolith microextraction coupled with HPLC[J]. journal of separation science,2011,34(6):675-680. |
| APA | Xiao PF,Bao CL,Jia QO,Su RY,Zhou WH,&Jia JB.(2011).Determination of nitroanilines in hair dye using polymer monolith microextraction coupled with HPLC.journal of separation science,34(6),675-680. |
| MLA | Xiao PF,et al."Determination of nitroanilines in hair dye using polymer monolith microextraction coupled with HPLC".journal of separation science 34.6(2011):675-680. |
入库方式： OAI收割
来源：长春应用化学研究所
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