Rhombic dodecahedral Fe(3)O(4): ionic liquid-modulated and microwave-assisted synthesis and their magnetic properties
文献类型:期刊论文
作者 | Li XY ; Liu DP ; Song SY ; Wang X ; Ge X ; Zhang HJ |
刊名 | crystengcomm
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出版日期 | 2011 |
卷号 | 13期号:20页码:6017-6020 |
关键词 | BLOCKING TEMPERATURE NANOPARTICLES CRYSTALLINE SHAPE DEPENDENCE PARTICLES EVOLUTION OXIDE |
ISSN号 | 1466-8033 |
通讯作者 | liu dp |
中文摘要 | rhombic dodecahedral (rd) fe(3)o(4) nanocrystals (ncs) were for the first time prepared via a rapid and facile microwave-assisted route in the presence of ionic liquids (ils). the reaction could be finished within 15 min at temperatures as low as 90 degrees c. a proper amount of ils played a key role in the synthesis of pure rd fe(3)o(4) ncs. in addition, the hmt-to-phenol molar ratio was also crucial for the growth of the rd fe(3)o(4) ncs. the phase structures, morphologies, and sizes of as-prepared products were investigated in detail by x-ray diffraction (xrd), scanning electron microscopy (sem), transmission electron microscopy (tem), and high-resolution tem (hrtem). the magnetic study reveals that the t(b) of the rd fe(3)o(4) ncs is found to be at 120 k, and the saturation magnetization is 86 emu g(-1) at room temperature. |
收录类别 | SCI收录期刊论文 |
语种 | 英语 |
公开日期 | 2012-06-11 |
源URL | [http://ir.ciac.jl.cn/handle/322003/44932] ![]() |
专题 | 长春应用化学研究所_长春应用化学研究所知识产出_期刊论文 |
推荐引用方式 GB/T 7714 | Li XY,Liu DP,Song SY,et al. Rhombic dodecahedral Fe(3)O(4): ionic liquid-modulated and microwave-assisted synthesis and their magnetic properties[J]. crystengcomm,2011,13(20):6017-6020. |
APA | Li XY,Liu DP,Song SY,Wang X,Ge X,&Zhang HJ.(2011).Rhombic dodecahedral Fe(3)O(4): ionic liquid-modulated and microwave-assisted synthesis and their magnetic properties.crystengcomm,13(20),6017-6020. |
MLA | Li XY,et al."Rhombic dodecahedral Fe(3)O(4): ionic liquid-modulated and microwave-assisted synthesis and their magnetic properties".crystengcomm 13.20(2011):6017-6020. |
入库方式: OAI收割
来源:长春应用化学研究所
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