SEPARATION AND DETERMINATION OF ALKALOIDS IN RHIZOMA CORYDALIS BY CAPILLARY ZONE ELECTROPHORESIS
文献类型：期刊论文
| 作者 | Li W ; Yang SB ; Pi ZF ; Song FR ; Liu ZQ |
| 刊名 | journal of liquid chromatography & related technologies
 |
| 出版日期 | 2011 |
| 卷号 | 34期号:12页码:1050-1061 |
| 关键词 | PROTOBERBERINE ALKALOIDS MEDICINAL PREPARATIONS MASS-SPECTROMETRY BERBERINE TETRAHYDROPALMATINE CHROMATOGRAPHY YANHUSUO |
| ISSN号 | 1082-6076 |
| 通讯作者 | liu zq |
| 中文摘要 | simple, rapid, reproducible capillary zone electrophoresis (cze) methods had been developed for the separation and determination of alkaloids in rhizoma corydalis and its preparation. four experimental parameters including electrolyte concentration, ph, organic modifier, and applied voltage were optimized. the optimum condition: 60mm disodium hydrogen phosphate and 55% (v/v) methanol, 24kv applied voltage, and temperature 30 degrees c. under the ph of running buffer (ph 4.27) and detection wavelength 214nm, tetrahydropalmatine was successfully separated. under the ph of running buffer (ph 2.80) and detection wavelength 254nm, palmatine was base line separated. the linearity between peak areas and the concentrations of the analytes were also investigated, and excellent linear behavior was obtained. |
| 收录类别 | SCI收录期刊论文 |
| 语种 | 英语 |
| WOS记录号 | WOS:000291807100008 |
| 公开日期 | 2012-06-11 |
| 源URL | [http://ir.ciac.jl.cn/handle/322003/44971]  |
| 专题 | 长春应用化学研究所_长春应用化学研究所知识产出_期刊论文 |
| 推荐引用方式 GB/T 7714 | Li W,Yang SB,Pi ZF,et al. SEPARATION AND DETERMINATION OF ALKALOIDS IN RHIZOMA CORYDALIS BY CAPILLARY ZONE ELECTROPHORESIS[J]. journal of liquid chromatography & related technologies,2011,34(12):1050-1061. |
| APA | Li W,Yang SB,Pi ZF,Song FR,&Liu ZQ.(2011).SEPARATION AND DETERMINATION OF ALKALOIDS IN RHIZOMA CORYDALIS BY CAPILLARY ZONE ELECTROPHORESIS.journal of liquid chromatography & related technologies,34(12),1050-1061. |
| MLA | Li W,et al."SEPARATION AND DETERMINATION OF ALKALOIDS IN RHIZOMA CORYDALIS BY CAPILLARY ZONE ELECTROPHORESIS".journal of liquid chromatography & related technologies 34.12(2011):1050-1061. |
入库方式： OAI收割
来源：长春应用化学研究所
浏览0
下载0
收藏0
其他版本
除非特别说明，本系统中所有内容都受版权保护，并保留所有权利。