A novel silica based click lysine anion exchanger for ion exchange chromatography
文献类型:期刊论文
作者 | Guo, Hongyue1; Chu, Changhu1; Li, Yan1; Yang, Bingcheng1; Liang, Xinmiao1,2 |
刊名 | analyst
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出版日期 | 2011 |
卷号 | 136期号:24页码:5302-5307 |
ISSN号 | 待补充 |
产权排序 | 2,5 |
通讯作者 | changhuchu ; bingchengyang |
中文摘要 | a novel silica based click lysine anion exchanger for ion exchange chromatography |
英文摘要 | ion chromatography (ic) is one of the most powerful analysis technologies for the determination of charged compounds. a novel click lysine stationary phase was prepared via cu(i) catalyzed alkyne-azide 1,3-dipolar cycloaddition (cuaac) and applied to the analysis of inorganic ions. the chromatographic evaluation demonstrated good performance (e.g. the plate number of thiocyanate is similar to 50 000 plates m(-1)) and effective separation ability for the common inorganic anions with aqueous na(2)so(4) eluent. the separation mechanism was observed to be mainly dominated by ion exchange interaction. the retention of these analytes is highly dependent on the ph value of eluent. compared with the lysine stationary phase prepared via the conventional manner, the click lysine exchanger demonstrated shorter retention time and better ion separation characteristics under the same chromatographic conditions, which is a great advantage for rapid separation and analysis of inorganic ions. |
WOS标题词 | science & technology ; physical sciences |
学科主题 | 物理化学 |
类目[WOS] | chemistry, analytical |
研究领域[WOS] | chemistry |
关键词[WOS] | performance liquid-chromatography ; stationary-phase ; inorganic anions ; reversed-phase ; efficient strategy ; acid ; separation ; chemistry ; column ; glycopeptides |
收录类别 | SCI |
语种 | 英语 |
WOS记录号 | WOS:000297223000030 |
公开日期 | 2012-07-09 |
源URL | [http://159.226.238.44/handle/321008/115652] ![]() |
专题 | 大连化学物理研究所_中国科学院大连化学物理研究所 |
作者单位 | 1.E China Univ Sci & Technol, Sch Pharm, Shanghai 200237, Peoples R China 2.Chinese Acad Sci, Dalian Inst Chem Phys, Dalian 116023, Peoples R China |
推荐引用方式 GB/T 7714 | Guo, Hongyue,Chu, Changhu,Li, Yan,et al. A novel silica based click lysine anion exchanger for ion exchange chromatography[J]. analyst,2011,136(24):5302-5307. |
APA | Guo, Hongyue,Chu, Changhu,Li, Yan,Yang, Bingcheng,&Liang, Xinmiao.(2011).A novel silica based click lysine anion exchanger for ion exchange chromatography.analyst,136(24),5302-5307. |
MLA | Guo, Hongyue,et al."A novel silica based click lysine anion exchanger for ion exchange chromatography".analyst 136.24(2011):5302-5307. |
入库方式: OAI收割
来源:大连化学物理研究所
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