A novel silver-coated solid-phase microextraction metal fiber based on electroless plating technique
文献类型：期刊论文
| 作者 | Jiang SX(蒋生祥) ; Liu X(刘霞); Jiang SX(蒋生祥)
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| 刊名 | Analytica Chimica Acta
 |
| 出版日期 | 2011 |
| 卷号 | 701页码:174-180 |
| 关键词 | Silver Electroless plating Solid-phase microextraction Gas chromatography Phthalate esters Polycyclic aromatic hydrocarbons |
| ISSN号 | 0003-2670 |
| 通讯作者 | 蒋生祥 |
| 中文摘要 | A novel silver-coated solid-phase microextraction fiber was prepared based on electroless plating technique. Good extraction performance of the fiber for model compounds including phthalate esters (dibutyl phthalate, dioctyl phthalate, dicyclohexyl phthalate and diallyl phthalate) and polycyclic aromatic hydrocarbons (naphthalene, fluorene, phenanthrene, fluoranthene) in aqueous solution was obtained. Under the optimized conditions (extraction temperature, extraction time, ionic strength and desorption temperature),the proposed SPME-GC method showed wide linear ranges with correlation coefficients (R2) ranging from 0.9745 to 0.9984. The limits of detection were at the range of 0.02 to 0.1µg L−1. Single fiber repeatability and fiber-to-fiber reproducibility as well as stability to acid, alkali and high temperature were studied and the results were all satisfactory. The method was applied successfully to the aqueous extracts of disposable paper cup and instant noodle barrel. Several kinds of analytes were detected and quantified. |
| 学科主题 | 分析化学与药物化学 |
| 收录类别 | SCI |
| 资助信息 | the National Natural Science Foundation of China (no. 20975105;no. 20905073;no. 20905072) |
| 语种 | 英语 |
| WOS记录号 | WOS:000294144400009 |
| 公开日期 | 2012-10-18 |
| 源URL | [http://210.77.64.217/handle/362003/1545]  |
| 专题 | 兰州化学物理研究所_中科院西北特色植物资源化学重点实验室/甘肃省天然药物重点实验室 |
| 通讯作者 | Jiang SX(蒋生祥); Jiang SX(蒋生祥) |
| 推荐引用方式 GB/T 7714 | Jiang SX,Liu X,Jiang SX. A novel silver-coated solid-phase microextraction metal fiber based on electroless plating technique[J]. Analytica Chimica Acta,2011,701:174-180. |
| APA | 蒋生祥,刘霞,&蒋生祥.(2011).A novel silver-coated solid-phase microextraction metal fiber based on electroless plating technique.Analytica Chimica Acta,701,174-180. |
| MLA | 蒋生祥,et al."A novel silver-coated solid-phase microextraction metal fiber based on electroless plating technique".Analytica Chimica Acta 701(2011):174-180. |
入库方式： OAI收割
来源：兰州化学物理研究所
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