Monitoring multi-class pesticide residues in fresh grape by hollow fibre sorptive extraction combined with gas chromatography–mass spectrometry
文献类型：期刊论文
| 作者 | Shi YP(师彦平) ; Shi YP(师彦平)
|
| 刊名 | Food Chemistry
 |
| 出版日期 | 2011 |
| 卷号 | 127页码:784-790 |
| 关键词 | Hollow fibre sorptive extraction Pesticides multi-residue Grape Gas chromatography–mass spectrometry |
| ISSN号 | 0308-8146 |
| 通讯作者 | 师彦平 |
| 中文摘要 | A fast and sensitive multi-residue analysis method is reported for simultaneous determination of 25 pesticides of chemical classes which are spiked into fresh grape. The sample pretreatment method involves extraction and clean-up in one step with SiO2 hollow fibre from 1.0 mL fresh grape slurry to minimise the matrix effects, and determination by gas chromatography–mass spectrometry with selective ion monitoring mode. The validation of the optimised method in terms of linearity, precision, recovery and repeatability showed that the proposed procedure is sensitive (the limits of detection were in the range of 0.0009–0.0084 lgmL 1 for 25 pesticides), precise and repeatable (average recoveries were between 61% and 108% with relative standard deviations from 4.0% to 12.4 %). The proposed method was also applied to the analysis of these groups of pesticides in fresh grape sample purchased from the local markets of Lanzhou (China), while no residues of the selected pesticides were detected in the sample. |
| 学科主题 | 分析化学与药物化学 |
| 收录类别 | SCI |
| 资助信息 | the National Nature Science Foundation of China (No. 20875095);National Key Technology Research and Development Program of China (No. 2007BAI37B05) |
| 语种 | 英语 |
| 公开日期 | 2012-10-18 |
| 源URL | [http://210.77.64.217/handle/362003/1517]  |
| 专题 | 兰州化学物理研究所_中科院西北特色植物资源化学重点实验室/甘肃省天然药物重点实验室 |
| 通讯作者 | Shi YP(师彦平); Shi YP(师彦平) |
| 推荐引用方式 GB/T 7714 | Shi YP,Shi YP. Monitoring multi-class pesticide residues in fresh grape by hollow fibre sorptive extraction combined with gas chromatography–mass spectrometry[J]. Food Chemistry,2011,127:784-790. |
| APA | 师彦平,&师彦平.(2011).Monitoring multi-class pesticide residues in fresh grape by hollow fibre sorptive extraction combined with gas chromatography–mass spectrometry.Food Chemistry,127,784-790. |
| MLA | 师彦平,et al."Monitoring multi-class pesticide residues in fresh grape by hollow fibre sorptive extraction combined with gas chromatography–mass spectrometry".Food Chemistry 127(2011):784-790. |
入库方式： OAI收割
来源：兰州化学物理研究所
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