Preparation of shuttle-like Sb2S3 nanorod-bundles via a solvothermal approach under alkaline condition
文献类型：期刊论文
| 作者 | Zhou HD(周惠娣) ; Chen JM(陈建敏); Chen L(陈磊); Wan HQ(万宏启)
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| 刊名 | Cryst. Res. Technol.
 |
| 出版日期 | 2010 |
| 卷号 | 45期号:2页码:178-182 |
| 关键词 | nanostructure semiconductor crystal growth |
| ISSN号 | 0232-1300 |
| 通讯作者 | 陈建敏 |
| 中文摘要 | Uniform shuttle-like Sb2S3 nanorod-bundles were synthesized via a polyvinylpyrrolidone (PVP) assisted solvothermal approach under alkaline condition, using antimony chloride (SbCl3) and thiourea (CH4N2S, Tu) as the starting materials in ethanol. The phase structure, composition and morphology of the product were characterized by means of X-ray diffraction (XRD), energy dispersive X-ray spectrometry (EDS), transmission electron microscopy (TEM), and high-resolution transmission electron microscopy (HRTEM). XRD and EDS results confirm that the synthesized Sb2S3 nanorod-bundles have an orthorhombic structure and an atomic ratio of 3:2 for S:Sb. TEM and HRTEM results show that the shuttle-like Sb2S3 bundles are composed of nanorods with a size distribution of 20-40 nm and growing along c-axis. Furthermore, experiments under different reaction conditions were carried out and the mechanism for the growth of nanorod-bundles was discussed. |
| 学科主题 | 材料科学与物理化学 |
| 收录类别 | SCI |
| 资助信息 | the “973” Program of China (Grant No. 2007CB607601);the Innovative Group Fund of National Natural Science Foundation of China (NNSFC, Grant No. 50421502) |
| 语种 | 英语 |
| WOS记录号 | WOS:000274872700012 |
| 公开日期 | 2012-09-28 |
| 源URL | [http://210.77.64.217/handle/362003/981]  |
| 专题 | 兰州化学物理研究所_固体润滑国家重点实验室 兰州化学物理研究所_先进润滑与防护材料研究发展中心 |
| 通讯作者 | Chen JM(陈建敏) |
| 推荐引用方式 GB/T 7714 | Zhou HD,Chen JM,Chen L,et al. Preparation of shuttle-like Sb2S3 nanorod-bundles via a solvothermal approach under alkaline condition[J]. Cryst. Res. Technol.,2010,45(2):178-182. |
| APA | 周惠娣,陈建敏,陈磊,&万宏启.(2010).Preparation of shuttle-like Sb2S3 nanorod-bundles via a solvothermal approach under alkaline condition.Cryst. Res. Technol.,45(2),178-182. |
| MLA | 周惠娣,et al."Preparation of shuttle-like Sb2S3 nanorod-bundles via a solvothermal approach under alkaline condition".Cryst. Res. Technol. 45.2(2010):178-182. |
入库方式： OAI收割
来源：兰州化学物理研究所
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