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  2. 兰州化学物理研究所
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  4. 固体润滑国家重点实验室
Synthesis of carbon nitride powder by selective etching of TiC0.3N0.7 in chlorine-containing atmosphere at moderate temperature

文献类型：期刊论文

作者Lv JJ(吕晋军); Lv JJ(吕晋军)
刊名Materials Chemistry and Physics
出版日期2010
卷号123页码:264-268
关键词Nitride Etching Fourier transform infrared spectroscopy (FTIR) X-ray photo-emission spectroscopy (XPS)
ISSN号0254-0584
通讯作者吕晋军
中文摘要We reported the synthesis of carbon nitride powder by extracting titanium from single inorganic pre-cursor TiC0.3N0.7 in chlorine-containing atmosphere at ambient pressure and temperature not exceeding500 ◦C. The TiC0.3N0.7 crystalline structure acted as a template, supplying active carbon and nitrogenatoms for carbon nitride when it was destroyed in chlorination. X-ray diffraction data showed that theobtained carbon nitride powders were amorphous, which was in good agreement with transmissionelectron microscope analysis. The composition and structure of carbon nitride powders were analyzedby employing Fourier transform infrared spectroscopy, Raman spectroscopy, and X-ray photoelectronspectroscopy. Results indicated that disorder structure was most likely for the carbon nitride powdersand the N content depended greatly on the chlorination temperature. Thermal analysis in flowing N2indicated that the mass loss started from 300 ◦C and the complete decomposition occurred at around650 ◦C, confirming the low thermal stability of the carbon nitride material.
学科主题材料科学与物理化学
收录类别SCI
语种英语
WOS记录号WOS:000279305800044
公开日期2012-09-28
源URL[http://210.77.64.217/handle/362003/1038]  
专题兰州化学物理研究所_固体润滑国家重点实验室
通讯作者Lv JJ(吕晋军); Lv JJ(吕晋军)
推荐引用方式
GB/T 7714		 Lv JJ,Lv JJ. Synthesis of carbon nitride powder by selective etching of TiC0.3N0.7 in chlorine-containing atmosphere at moderate temperature[J]. Materials Chemistry and Physics,2010,123:264-268.
APA 吕晋军,&吕晋军.(2010).Synthesis of carbon nitride powder by selective etching of TiC0.3N0.7 in chlorine-containing atmosphere at moderate temperature.Materials Chemistry and Physics,123,264-268.
MLA 吕晋军,et al."Synthesis of carbon nitride powder by selective etching of TiC0.3N0.7 in chlorine-containing atmosphere at moderate temperature".Materials Chemistry and Physics 123(2010):264-268.

入库方式： OAI收割

来源：兰州化学物理研究所

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