Application of preparative high-speed countercurrent chromatography for separation of elatine from Delphinium shawurense
文献类型：期刊论文
| 作者 | Yang Yi; Gu Dongyu; Wu Hankui; Aisa Haji Akber ; Zhang Tianyou; Ito Yoichiro
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| 刊名 | JOURNAL OF LIQUID CHROMATOGRAPHY & RELATED TECHNOLOGIES
 |
| 出版日期 | 2008 |
| 卷号 | 31期号:19页码:3012-3019 |
| 关键词 | Delphinium shawurense elatine high speed countercurrent chromatography (HSCCC) |
| ISSN号 | 10826076 |
| 通讯作者 | Aisa, HA |
| 英文摘要 | Preparative separation of elatine in Delphinium shawurense was achieved for the first time using high speed countercurrent chromatography (HSCCC). The separation was performed with a solvent system composed of ethyl acetate-chloroform-methanol-water (3:0.1:2:3, v/v) using the lower organic phase as a mobile phase under a revolution speed of 800 rpm. This yielded 72 mg of elatine at over 97% purity with an approximately 95% recovery. The chemical structure was identified by MS and NMR. |
| 收录类别 | EI |
| WOS记录号 | WOS:000259695300009 |
| 公开日期 | 2012-11-29 |
| 源URL | [http://ir.xjipc.cas.cn/handle/365002/2079]  |
| 专题 | 新疆理化技术研究所_资源化学研究室 |
| 作者单位 | Chinese Acad Sci, Xinjiang Key Lab Plant Resources & Nat Prod Chem, Xinjiang Tech Inst Phys & Chem, Urumqi, Peoples R China;Chinese Acad Sci, Grad Univ, Beijing, Peoples R China;Beijing Inst New Technol, Beijing, Peoples R China; NHLBI, Ctr Biochem & Biophys, NIH, Bethesda, MD 20892 USA |
| 推荐引用方式 GB/T 7714 | Yang Yi,Gu Dongyu,Wu Hankui,et al. Application of preparative high-speed countercurrent chromatography for separation of elatine from Delphinium shawurense[J]. JOURNAL OF LIQUID CHROMATOGRAPHY & RELATED TECHNOLOGIES,2008,31(19):3012-3019. |
| APA | Yang Yi,Gu Dongyu,Wu Hankui,Aisa Haji Akber,Zhang Tianyou,&Ito Yoichiro.(2008).Application of preparative high-speed countercurrent chromatography for separation of elatine from Delphinium shawurense.JOURNAL OF LIQUID CHROMATOGRAPHY & RELATED TECHNOLOGIES,31(19),3012-3019. |
| MLA | Yang Yi,et al."Application of preparative high-speed countercurrent chromatography for separation of elatine from Delphinium shawurense".JOURNAL OF LIQUID CHROMATOGRAPHY & RELATED TECHNOLOGIES 31.19(2008):3012-3019. |
入库方式： OAI收割
来源：新疆理化技术研究所
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