Constant current etching of gold tips suitable for tip-enhanced Raman spectroscopy
文献类型:期刊论文
作者 | Zengli Huang(黄增立)![]() ![]() ![]() ![]() ![]() ![]() |
刊名 | Review of scientific instruments
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出版日期 | 2012-10 |
卷号 | 83期号:10 |
通讯作者 | Ke Xu(徐科) |
英文摘要 | We introduce a setup and method to produce gold tips that are suitable for tip-enhanced Raman spectroscopy by using a single step constant current electrochemical etch. The etching process is fully automated with only three preset parameters: the etching current, the reference voltage and the immersed length of gold wires. By optimizing these parameters, reproducible high quality tips with smooth surface and a radius curvature of about 20 nm can be formed. Tips prepared with this method were examined by tip-enhanced Raman spectroscopy experiments on the samples of single-wall carbon nanotube, p-aminothiophenol, and graphene. In the Raman mapping of single-wall carbon nanotubes, the spatial resolution is about 15 nm. |
收录类别 | SCI |
WOS记录号 | WOS:000311562500033 |
公开日期 | 2013-01-22 |
源URL | [http://58.210.77.100/handle/332007/1045] ![]() |
专题 | 苏州纳米技术与纳米仿生研究所_测试分析平台 |
通讯作者 | Ke Xu(徐科); Ke Xu(徐科) |
推荐引用方式 GB/T 7714 | Zengli Huang,Gengzhao Xu,Ke Xu,et al. Constant current etching of gold tips suitable for tip-enhanced Raman spectroscopy[J]. Review of scientific instruments,2012,83(10). |
APA | Zengli Huang,Gengzhao Xu,Ke Xu,Ke Xu,Haijian Zhong,&Yingmin Fan.(2012).Constant current etching of gold tips suitable for tip-enhanced Raman spectroscopy.Review of scientific instruments,83(10). |
MLA | Zengli Huang,et al."Constant current etching of gold tips suitable for tip-enhanced Raman spectroscopy".Review of scientific instruments 83.10(2012). |
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