Study of 2-iodo-3-(phenylsulfinyl)-2-propen-1-ol and its analogues by self-chemical ionization mass spectrometry
文献类型:期刊论文
作者 | Zhang F(张芳) ; Guo YL(郭寅龙) ; Wei Q(魏崎) ; Ma SM(麻生明) |
刊名 | Chin. J. Chem.
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出版日期 | 2001 |
卷号 | 19期号:9页码:851-855 |
ISSN号 | 1001-604X |
其他题名 | 2-碘代-3-(苯亚砜基)-2-丙烯-1-醇及其衍生物的SCI质谱研究 |
通讯作者 | 郭寅龙 ; 麻生明 |
英文摘要 | The self-chemical ionization (SCI) in quadrupole mass spectrometry was developed to determine the structure of (E) -2-iodo-3-(phenylsulfinyl)-2-propen-1-ol and its 6 analogues. Some techniques that increase the sample quantity and heating speed and shorten vaporization time to obtain high pressure in the ion source were applied to increase the chance of ionmolecule reactions. The structures of these compounds were identified by mass spectral data of MH+ and some characteristic fragment ions. Compared with the mass spectra for 2-io-do-3-(phenylsulfinyl)-2-propen-1-ols obtained in electron impact ionization (EI), SCI showed more information, in particular, an imporovement in amount of informaion at the high mass area. The absence of reagent gas makes the spectrum clean and simple. |
学科主题 | 有机化学 |
收录类别 | SCI |
原文出处 | http://dx.doi.org/10.1002/cjoc.20010190908 |
语种 | 英语 |
WOS记录号 | WOS:000171475700007 |
公开日期 | 2013-01-15 |
源URL | [http://202.127.28.38/handle/331003/11844] ![]() |
专题 | 上海有机化学研究所_金属有机化学国家重点实验室 |
推荐引用方式 GB/T 7714 | Zhang F,Guo YL,Wei Q,et al. Study of 2-iodo-3-(phenylsulfinyl)-2-propen-1-ol and its analogues by self-chemical ionization mass spectrometry[J]. Chin. J. Chem.,2001,19(9):851-855. |
APA | 张芳,郭寅龙,魏崎,&麻生明.(2001).Study of 2-iodo-3-(phenylsulfinyl)-2-propen-1-ol and its analogues by self-chemical ionization mass spectrometry.Chin. J. Chem.,19(9),851-855. |
MLA | 张芳,et al."Study of 2-iodo-3-(phenylsulfinyl)-2-propen-1-ol and its analogues by self-chemical ionization mass spectrometry".Chin. J. Chem. 19.9(2001):851-855. |
入库方式: OAI收割
来源:上海有机化学研究所
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