Synthesis and crystal structure of {Cd(hmbdc)(H2O)(3)}center dot 2H(2)O (n)
文献类型:期刊论文
作者 | Y. H. Hu ; Y. Wang ; Z. W. Wang ; Y. Z. Li ; H. G. Zheng |
刊名 | Chinese Journal of Structural Chemistry
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出版日期 | 2007 |
卷号 | 26期号:4页码:423-426 |
关键词 | Cd(II) complex crystal structure hydrogen bond network structure complexes network solids |
ISSN号 | 0254-5861 |
中文摘要 | A novel coordination polymer [{Cd(hmbdc)(H2O)(3)}center dot 2H(2)O](n) (hmbdc= 5-hydroxyisophthalic acid) has been synthesized and characterized by elemental analysis, IR spectra and single-crystal X-ray diffraction. The crystal belongs to monoclinic, space group P2(1)/c, with a 9.599(3), b = 18.699(5), c = 7.557(2) angstrom, beta = 108.198(4)degrees, V=1288.6(6) angstrom(3), Z = 4, M-r = 3 82.60, D-c 1.972 g/cm(3), F(000) = 760, mu = 1.740, the final R = 0.0555 and wR = 0.0995 for 1732 observed reflections with I > 2 sigma(I). The structural analysis shows that the intermolecular hydrogen bonds and pi-pi interactions result in a three-dimensional supramolecular framework. |
语种 | 英语 |
公开日期 | 2013-04-01 |
源URL | [http://ir.fjirsm.ac.cn/handle/350002/6294] ![]() |
专题 | 福建物质结构研究所_中科院福建物质结构研究所_期刊论文 |
推荐引用方式 GB/T 7714 | Y. H. Hu,Y. Wang,Z. W. Wang,et al. Synthesis and crystal structure of {Cd(hmbdc)(H2O)(3)}center dot 2H(2)O (n)[J]. Chinese Journal of Structural Chemistry,2007,26(4):423-426. |
APA | Y. H. Hu,Y. Wang,Z. W. Wang,Y. Z. Li,&H. G. Zheng.(2007).Synthesis and crystal structure of {Cd(hmbdc)(H2O)(3)}center dot 2H(2)O (n).Chinese Journal of Structural Chemistry,26(4),423-426. |
MLA | Y. H. Hu,et al."Synthesis and crystal structure of {Cd(hmbdc)(H2O)(3)}center dot 2H(2)O (n)".Chinese Journal of Structural Chemistry 26.4(2007):423-426. |
入库方式: OAI收割
来源:福建物质结构研究所
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