Synthesis and crystal structure of a 2-D hydrogen-bonded supramolecular Network { Cu-4(OH)(4)(2,2 '-bpy)(4)(bqdc) center dot 2ClO(4)}n
文献类型：期刊论文
| 作者 | J. H. Luo ; C. Lian ; C. Y. Yue ; F. L. Jiang ; M. C. Hong |
| 刊名 | Chinese Journal of Structural Chemistry
 |
| 出版日期 | 2007 |
| 卷号 | 26期号:6页码:654-658 |
| 关键词 | hydrothermal method copper(II) crystal structure supramolecular pi-pi stacking complexes architectures ligands |
| ISSN号 | 0254-5861 |
| 中文摘要 | The title compound {[Cu-4(OH)(4)(2,2'-bpy)(4)(bqdc)]center dot 2ClO(4)}(n) 1(bqdc = 2,2'-biquinoline-4,4'-dicarboxylic acid) has been synthesized by hydrothermal method. Its crystal structure is of triclinic, space group P (1) over bar with a = 7.6561(5), b = 12-4652(8), c = 15.7501(10) angstrom, alpha = 80.0480(10), beta = 87.7900(10), gamma = 74.0800(1)degrees, V = 1423.65(16) angstrom(3), Z = 2, C30H23ClN5O8Cu2, M-r = 744.06, D-c = 1.736 g/cm(3), mu = 1.651 mm(-1), F(000) = 754, the final R = 0.0421 and wR = 0.1163 for 4973 observed reflections with I > 2 sigma(I). In 1, tetra-copper chair-like clusters of [Cu-4(OH)(4)(2,2'-bpy)(4)](4+) are connected by bqdc ligands to form one-dimensional chains, which are further connected by hydrogen bonds to generate a two-dimensional supramolecular network. |
| 语种 | 英语 |
| 公开日期 | 2013-04-01 |
| 源URL | [http://ir.fjirsm.ac.cn/handle/350002/6514]  |
| 专题 | 福建物质结构研究所_中科院福建物质结构研究所_期刊论文 |
| 推荐引用方式 GB/T 7714 | J. H. Luo,C. Lian,C. Y. Yue,et al. Synthesis and crystal structure of a 2-D hydrogen-bonded supramolecular Network { Cu-4(OH)(4)(2,2 '-bpy)(4)(bqdc) center dot 2ClO(4)}n[J]. Chinese Journal of Structural Chemistry,2007,26(6):654-658. |
| APA | J. H. Luo,C. Lian,C. Y. Yue,F. L. Jiang,&M. C. Hong.(2007).Synthesis and crystal structure of a 2-D hydrogen-bonded supramolecular Network { Cu-4(OH)(4)(2,2 '-bpy)(4)(bqdc) center dot 2ClO(4)}n.Chinese Journal of Structural Chemistry,26(6),654-658. |
| MLA | J. H. Luo,et al."Synthesis and crystal structure of a 2-D hydrogen-bonded supramolecular Network { Cu-4(OH)(4)(2,2 '-bpy)(4)(bqdc) center dot 2ClO(4)}n".Chinese Journal of Structural Chemistry 26.6(2007):654-658. |
入库方式： OAI收割
来源：福建物质结构研究所
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