Synthesis and crystal structure of a Mo-S cluster compound coordinated by isonicotinate
文献类型：期刊论文
| 作者 | Y. Y. Qin ; Z. J. Li ; Y. Kang ; J. Zhang ; J. K. Cheng ; Y. G. Yao |
| 刊名 | Chinese Journal of Structural Chemistry
 |
| 出版日期 | 2007 |
| 卷号 | 26期号:9页码:1043-1046 |
| 关键词 | molybdenum cluster synthesis crystal structure molybdenum complexes |
| ISSN号 | 0254-5861 |
| 中文摘要 | A cluster compound, MO3S4(DTP)(3)(IN)(Py)center dot EtOH I (DTP = diethyl dithiophosphate, IN = isonicotinate) has been rationally synthesized and characterized by single-crystal X-ray diffraction. The crystal belongs to the triclinic system, space group P ((1)) over bar with a = 13.6345(2), b = 13.7805(2), c = 14.5400(1) angstrom, alpha = 107.078(1), beta = 113.380(1), gamma = 96.310(1)degrees, C25H45Mo3N2O9P3S10 M-r = 1218.96, V = 2315.75(5) angstrom(3), Z = 2, D-c = 1.748 g/cm(3), mu = 1.399, F(000) = 1224, R = 0.0425 and wR = 0.1144 for 6335 observed reflections (I > 2 sigma(I)). P-31 NMR spectrum has been measured with the resonance 110.050 and 108.7 83 (2:1). |
| 语种 | 英语 |
| 公开日期 | 2013-04-01 |
| 源URL | [http://ir.fjirsm.ac.cn/handle/350002/6570]  |
| 专题 | 福建物质结构研究所_中科院福建物质结构研究所_期刊论文 |
| 推荐引用方式 GB/T 7714 | Y. Y. Qin,Z. J. Li,Y. Kang,et al. Synthesis and crystal structure of a Mo-S cluster compound coordinated by isonicotinate[J]. Chinese Journal of Structural Chemistry,2007,26(9):1043-1046. |
| APA | Y. Y. Qin,Z. J. Li,Y. Kang,J. Zhang,J. K. Cheng,&Y. G. Yao.(2007).Synthesis and crystal structure of a Mo-S cluster compound coordinated by isonicotinate.Chinese Journal of Structural Chemistry,26(9),1043-1046. |
| MLA | Y. Y. Qin,et al."Synthesis and crystal structure of a Mo-S cluster compound coordinated by isonicotinate".Chinese Journal of Structural Chemistry 26.9(2007):1043-1046. |
入库方式： OAI收割
来源：福建物质结构研究所
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