Capillary Electrophoresis Coupled with Electrochemiluminescence for the Facile Separation and Determination of Salbutamol and Clenbuterol in Urine
文献类型：期刊论文
| 作者 | Bao Y ; Yang F ; Yang XR |
| 刊名 | electroanalysis
 |
| 出版日期 | 2012 |
| 卷号 | 24期号:7页码:1597-1603 |
| 关键词 | PERFORMANCE LIQUID-CHROMATOGRAPHY IONIC LIQUIDS ELECTROGENERATED CHEMILUMINESCENCE ELECTROCHEMICAL DETECTION CE-ELECTROCHEMILUMINESCENCE SOLID-PHASE CYCLODEXTRIN EXTRACTION ALKALOIDS MEDICINE |
| ISSN号 | 1040-0397 |
| 通讯作者 | yang xr |
| 中文摘要 | a capillary electrophoresis coupled with tris(2,2'-bipyridyl) ruthenium(ii) (ru(bpy)32+) electrochemiluminescence detection system was developed to determine salbutamol and clenbuterol in urine. some factors that affected the performances of separation and detection were investigated. under the optimized conditions, one single quantitative analysis of salbutamol and clenbuterol was achieved at a separation voltage of 15 kv within 9 min, and the lods (s/n=3) and loqs (s/n=10) of salbutamol and clenbuterol were 8.43x10-8 mol/l, 2.61x10-7 mol/l and 2.73x10-7 mol/l, 8.21x10-7 mol/l, respectively. the recovery obtained from the analysis of spiked urine samples was between 88.6?% and 104.7?% with rsds lower than 6.70?%. the method was successfully applied to determine salbutamol and clenbuterol in urine samples. |
| 收录类别 | SCI收录期刊论文 |
| 语种 | 英语 |
| WOS记录号 | WOS:000305999200015 |
| 公开日期 | 2013-05-20 |
| 源URL | [http://ir.ciac.jl.cn/handle/322003/48071]  |
| 专题 | 长春应用化学研究所_长春应用化学研究所知识产出_期刊论文 |
| 推荐引用方式 GB/T 7714 | Bao Y,Yang F,Yang XR. Capillary Electrophoresis Coupled with Electrochemiluminescence for the Facile Separation and Determination of Salbutamol and Clenbuterol in Urine[J]. electroanalysis,2012,24(7):1597-1603. |
| APA | Bao Y,Yang F,&Yang XR.(2012).Capillary Electrophoresis Coupled with Electrochemiluminescence for the Facile Separation and Determination of Salbutamol and Clenbuterol in Urine.electroanalysis,24(7),1597-1603. |
| MLA | Bao Y,et al."Capillary Electrophoresis Coupled with Electrochemiluminescence for the Facile Separation and Determination of Salbutamol and Clenbuterol in Urine".electroanalysis 24.7(2012):1597-1603. |
入库方式： OAI收割
来源：长春应用化学研究所
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