Effects of surfactants on the structure and crystal growth behavior of Sm2Zr2O7 nanocrystalline
文献类型:期刊论文
作者 | Wang CJ ; Wang Y ; Cheng YL ; Huang WZ ; Zou BL ; Cao XQ |
刊名 | powder technology
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出版日期 | 2012 |
卷号 | 225页码:130-135 |
关键词 | THERMAL-EXPANSION CERIUM OXIDE PYROCHLORE ZIRCONIA CONDUCTIVITY TEMPERATURE CERAMICS POWDER |
ISSN号 | 0032-5910 |
通讯作者 | cao xq |
中文摘要 | sm2zr2o7 nanocrystallines were synthesized via hydrothermal method using polyethyleneglycol (peg), cetyltrimethyl ammonium bromide (ctab) and sodium dodecylbenzene sulfonate (sobs) as surfactants, respectively. the effects of surfactants on the structural evolution and the crystal growth of sm2zr2o7 were investigated by x-ray diffraction (xrd), thermogravimetric analysis and differential scanning calorimeter (tg/dsc). raman spectroscopy, field emission scanning electron microscope (fesem) and high resolution transmission electron microscopy (hrtem), separately. the as-prepared products have a spherical morphology, and the average particle sizes are in the range of 4-9 nm. the structure transition from fluorite to pyrochlore structure occurred at 1300 degrees c with peg and sdbs, which can be restrained by adding ctab. the activation energy of crystal growth is significantly dependent on the surfactants, which is in the order of sdbs>peg>ctab. moreover, the effects of surfactant on the sintering-resistance property of the products are also discussed. (c) 2012 elsevier b.v. all rights reserved. |
收录类别 | SCI收录期刊论文 |
语种 | 英语 |
WOS记录号 | WOS:000305380400017 |
公开日期 | 2013-05-20 |
源URL | [http://ir.ciac.jl.cn/handle/322003/48079] ![]() |
专题 | 长春应用化学研究所_长春应用化学研究所知识产出_期刊论文 |
推荐引用方式 GB/T 7714 | Wang CJ,Wang Y,Cheng YL,et al. Effects of surfactants on the structure and crystal growth behavior of Sm2Zr2O7 nanocrystalline[J]. powder technology,2012,225:130-135. |
APA | Wang CJ,Wang Y,Cheng YL,Huang WZ,Zou BL,&Cao XQ.(2012).Effects of surfactants on the structure and crystal growth behavior of Sm2Zr2O7 nanocrystalline.powder technology,225,130-135. |
MLA | Wang CJ,et al."Effects of surfactants on the structure and crystal growth behavior of Sm2Zr2O7 nanocrystalline".powder technology 225(2012):130-135. |
入库方式: OAI收割
来源:长春应用化学研究所
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