Reactions of 4-ethoxy-1,1,1-trifluorobut-3-en-2-one with diethyl malonate anion: synthesis and crystal structures of fluorinated organo alkali-metal complexes
文献类型:期刊论文
作者 | Song T(宋涛) ; Liu L(刘磊) ; Zhao JW(赵经纬) ; Jiang HL(蒋慧玲) ; Zhu SZ(朱仕正) ; Xu LZ(徐良忠) |
刊名 | Tetrahedron
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出版日期 | 2012 |
卷号 | 68期号:27-28页码:5677-5682 |
ISSN号 | 0040-4020 |
其他题名 | 三氟乙酰基乙烯基乙醚与丙二酸二乙酯的反应以及含氟有机碱金属配合物的晶体结构研究 |
通讯作者 | 朱仕正 |
英文摘要 | At room temperature, 4-ethoxy-1,1,1-trifluorobut-3-en-2-one reacted with alkali metal salts of diethyl malonate to give two kinds of complexes. One is the solvent molecule-involved complexes, and the other is a sheer ion aggregates composed by alkali metal cation and carbanion. Both crystals are fully characterized by spectroscopic methods and single crystal X-ray diffraction analyses. (c) 2012 Elsevier Ltd. All rights reserved. |
学科主题 | 氟化学 |
收录类别 | SCI |
原文出处 | http://dx.doi.org/10.1016/j.tet.2012.04.029 |
语种 | 英语 |
WOS记录号 | WOS:000306350800044 |
公开日期 | 2013-08-23 |
源URL | [http://202.127.28.38/handle/331003/28229] ![]() |
专题 | 上海有机化学研究所_中科院有机氟化学重点实验室 |
推荐引用方式 GB/T 7714 | Song T,Liu L,Zhao JW,et al. Reactions of 4-ethoxy-1,1,1-trifluorobut-3-en-2-one with diethyl malonate anion: synthesis and crystal structures of fluorinated organo alkali-metal complexes[J]. Tetrahedron,2012,68(27-28):5677-5682. |
APA | 宋涛,刘磊,赵经纬,蒋慧玲,朱仕正,&徐良忠.(2012).Reactions of 4-ethoxy-1,1,1-trifluorobut-3-en-2-one with diethyl malonate anion: synthesis and crystal structures of fluorinated organo alkali-metal complexes.Tetrahedron,68(27-28),5677-5682. |
MLA | 宋涛,et al."Reactions of 4-ethoxy-1,1,1-trifluorobut-3-en-2-one with diethyl malonate anion: synthesis and crystal structures of fluorinated organo alkali-metal complexes".Tetrahedron 68.27-28(2012):5677-5682. |
入库方式: OAI收割
来源:上海有机化学研究所
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