Effect of Zr/Ce molar ratio on the structure of powders and Zr1-xCexO2 coatings on quartz fiber reinforced polyimide matrix composites via sol-gel process
文献类型:期刊论文
作者 | Huang WZ ; Wang CJ ; Yang JL ; Zou BL ; Meng XS ; Wang Y ; Cao XQ ; Wang Z |
刊名 | journal of sol-gel science and technology |
出版日期 | 2012 |
卷号 | 61期号:1页码:213-223 |
ISSN号 | 0928-0707 |
关键词 | THERMAL BARRIER COATINGS ZIRCONIA RESISTANCE NANOCRYSTALS CERAMICS BEHAVIOR EROSION CITRATE ALLOYS OXIDES |
通讯作者 | cao xq |
中文摘要 | in this investigation, zr1-xcexo2 coatings were fabricated on quartz fiber reinforced polyimide matrix composites via sol-gel process at 400 degrees c. the phase evolution, structural and morphological characteristic of specimens were investigated by differential scanning calorimetric, fourier transform infrared spectroscopy, powder x-ray diffraction and scanning electron microscopy. the significant phase evolution of final powders with the decreasing zr/ce molar ratio could be observed as follows: tetragonal (t') -> cubic + tetragonal (t') -> tetragonal (t ''). bet specific surface areas of powders exhibited a decreased tendency with the increasing calcination temperature as well as the decreasing zr/ce molar ratio. the average crystallite size and the mean particle size increased with the elevated calcination temperature, while the particle size also increased with the increase in ce content. the progressive addition of ce could promote the sintering process and the densification of coating. morphologies of coatings changed with the variation of the zr/ce molar ratio. the results indicate that zr0.75ce0.25o2 coating with the zr/ce molar ratio of 3 is a stable uniform coating with excellent adhesion. |
收录类别 | SCI收录期刊论文 |
语种 | 英语 |
WOS记录号 | WOS:000299083700031 |
公开日期 | 2013-09-03 |
源URL | [http://ir.ciac.jl.cn/handle/322003/48739] |
专题 | 长春应用化学研究所_长春应用化学研究所知识产出_期刊论文 |
推荐引用方式 GB/T 7714 | Huang WZ,Wang CJ,Yang JL,et al. Effect of Zr/Ce molar ratio on the structure of powders and Zr1-xCexO2 coatings on quartz fiber reinforced polyimide matrix composites via sol-gel process[J]. journal of sol-gel science and technology,2012,61(1):213-223. |
APA | Huang WZ.,Wang CJ.,Yang JL.,Zou BL.,Meng XS.,...&Wang Z.(2012).Effect of Zr/Ce molar ratio on the structure of powders and Zr1-xCexO2 coatings on quartz fiber reinforced polyimide matrix composites via sol-gel process.journal of sol-gel science and technology,61(1),213-223. |
MLA | Huang WZ,et al."Effect of Zr/Ce molar ratio on the structure of powders and Zr1-xCexO2 coatings on quartz fiber reinforced polyimide matrix composites via sol-gel process".journal of sol-gel science and technology 61.1(2012):213-223. |
入库方式: OAI收割
来源:长春应用化学研究所
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