Determination of absolute configuration using heavy atom based co-crystallization method: Halogen atom effects
文献类型:期刊论文
作者 | Wang, Jian-Rong2![]() ![]() |
刊名 | JOURNAL OF MOLECULAR STRUCTURE
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出版日期 | 2016-09-05 |
卷号 | 1119页码:269-275 |
关键词 | Absolute configuration Co-crystallization Heavy atom Cholestanol L-Ascorbic acid Single-crystal X-ray diffraction |
ISSN号 | 0022-2860 |
DOI | 10.1016/j.molstruc.2016.04.084 |
文献子类 | Article |
英文摘要 | Heavy atom (chloride, bromide, and iodide) based co-crystals for determination of absolute configuration (AC) for chiral molecules were synthesized and evaluated. Co-crystals of cholestanol and L-ascorbic acid were analysed and the effects and potential benefits of varying the heavy atom are discussed. Changing the halogen atoms (chloride, bromide, or iodide) affects the co-crystal formation, X-ray absorption, and anomalous dispersion, and hence the ability to determine AC. (C) 2016 Elsevier B.V. All rights reserved. |
WOS关键词 | ORGANIC-SYNTHESIS ; CO-CRYSTAL ; CRYSTALLOGRAPHY |
资助项目 | National Natural Science Foundation of China[81273479] ; National Natural Science Foundation of China[81402898] ; CAS Key Technology Talent Program[00000000] ; Youth Innovation Promotion Association CAS[2016257] |
WOS研究方向 | Chemistry |
语种 | 英语 |
WOS记录号 | WOS:000378360000032 |
出版者 | ELSEVIER SCIENCE BV |
源URL | [http://119.78.100.183/handle/2S10ELR8/275900] ![]() |
专题 | 药物质量控制与固体化学研究中心 |
通讯作者 | Mei, Xuefeng |
作者单位 | 1.Univ Sci & Technol China, Nano Sci & Technol Inst, Suzhou 215123, Jiangsu, Peoples R China 2.Chinese Acad Sci, Shanghai Inst Mat Med, Pharmaceut Analyt & Solid State Chem Res Ctr, Shanghai 201203, Peoples R China; |
推荐引用方式 GB/T 7714 | Wang, Jian-Rong,Fan, Xiaowu,Ding, Qiaoce,et al. Determination of absolute configuration using heavy atom based co-crystallization method: Halogen atom effects[J]. JOURNAL OF MOLECULAR STRUCTURE,2016,1119:269-275. |
APA | Wang, Jian-Rong,Fan, Xiaowu,Ding, Qiaoce,&Mei, Xuefeng.(2016).Determination of absolute configuration using heavy atom based co-crystallization method: Halogen atom effects.JOURNAL OF MOLECULAR STRUCTURE,1119,269-275. |
MLA | Wang, Jian-Rong,et al."Determination of absolute configuration using heavy atom based co-crystallization method: Halogen atom effects".JOURNAL OF MOLECULAR STRUCTURE 1119(2016):269-275. |
入库方式: OAI收割
来源:上海药物研究所
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