Selective crystallization of vitamin D-3 for the preparation of novel conformational polymorphs with distinctive chemical stability
文献类型：期刊论文
| 作者 | Wang, Jian-Rong ; Zhu, Bingqing; Yu, Qihui; Mei, Xuefeng
|
| 刊名 | CRYSTENGCOMM
 |
| 出版日期 | 2016 |
| 卷号 | 18期号:7页码:1101-1104 |
| ISSN号 | 1466-8033 |
| DOI | 10.1039/c5ce02431e |
| 文献子类 | Article |
| 英文摘要 | A new conformational polymorph of VD3 containing a pure a conformer was prepared and fully characterized. Chemical stability and hygroscopicity are compared with the marketed solid-state form (form A, two conformers alpha/beta, 1 : 1). The results indicate that crystallization of VD3 needs to be controlled to avoid the unstable polymorph. |
| WOS关键词 | SOLID-STATE NMR ; 1-ALPHA,25-DIHYDROXYVITAMIN-D3 ; COCRYSTAL ; FORMS |
| 资助项目 | National Natural Science Foundation of China[81273479] ; National Natural Science Foundation of China[81402898] ; CAS Key Technology Talent Program[00000000] ; Youth Innovation Promotion Association CAS[00000000] |
| WOS研究方向 | Chemistry ; Crystallography |
| 语种 | 英语 |
| WOS记录号 | WOS:000369670800003 |
| 出版者 | ROYAL SOC CHEMISTRY |
| 源URL | [http://119.78.100.183/handle/2S10ELR8/276248]  |
| 专题 | 药物质量控制与固体化学研究中心 |
| 通讯作者 | Mei, Xuefeng |
| 作者单位 | Chinese Acad Sci, Shanghai Inst Mat Med, Pharmaceut Analyt & Solid State Chem Res Ctr, Shanghai 201203, Peoples R China |
| 推荐引用方式 GB/T 7714 | Wang, Jian-Rong,Zhu, Bingqing,Yu, Qihui,et al. Selective crystallization of vitamin D-3 for the preparation of novel conformational polymorphs with distinctive chemical stability[J]. CRYSTENGCOMM,2016,18(7):1101-1104. |
| APA | Wang, Jian-Rong,Zhu, Bingqing,Yu, Qihui,&Mei, Xuefeng.(2016).Selective crystallization of vitamin D-3 for the preparation of novel conformational polymorphs with distinctive chemical stability.CRYSTENGCOMM,18(7),1101-1104. |
| MLA | Wang, Jian-Rong,et al."Selective crystallization of vitamin D-3 for the preparation of novel conformational polymorphs with distinctive chemical stability".CRYSTENGCOMM 18.7(2016):1101-1104. |
入库方式： OAI收割
来源：上海药物研究所
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