Efficient Determination of the Enantiomeric Purity and Absolute Configuration of Flavanones by Using (S)-3,3 '-Dibromo-1,1 '-bi-2-naphthol as a Chiral Solvating Agent
文献类型：期刊论文
| 作者 | Du, Guoxin2,3; Li, Yisu1,3; Ma, Shunan2; Wang, Rui2; Li, Bo3; Guo, Fujiang2; Zhu, Weiliang3 ; Li, Yiming2
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| 刊名 | JOURNAL OF NATURAL PRODUCTS
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| 出版日期 | 2015-12 |
| 卷号 | 78期号:12页码:2968-2974 |
| ISSN号 | 0163-3864 |
| DOI | 10.1021/acs.jnatprod.5b00690 |
| 文献子类 | Article |
| 英文摘要 | The enantiomeric purity and absolute configuration of flavanones were first determined using (S)-3,3'-dibromo-1,1'-bi-2-naphthol as a chiral solvating agent by means of H-1 NMR spectroscopy. The enantiomeric purity results closely matched those based on chiral HPLC analysis. |
| WOS关键词 | NMR-SPECTROSCOPY ; CIRCULAR-DICHROISM ; CARBOXYLIC-ACIDS ; PRIMARY AMINES ; SHIFT-REAGENT ; HYDROXY-ACIDS ; ASSIGNMENT ; ENANTIODIFFERENTIATION ; DISCRIMINATION ; (S)-BINOL |
| 资助项目 | National Natural Science Foundation of China[81173518] ; Eastern Scholar Tracking Program of Shanghai Municipal Education Commission[2012-90] ; National High Technology Research and Development Program of China (863 program)[2013AA093003] ; International Collaboration Project[2014DFA31130] ; Program of Shanghai E-institute of Bioactive Constituents in Traditional Chinese Medicine[00000000] |
| WOS研究方向 | Plant Sciences ; Pharmacology & Pharmacy |
| 语种 | 英语 |
| WOS记录号 | WOS:000367562600013 |
| 出版者 | AMER CHEMICAL SOC |
| 源URL | [http://119.78.100.183/handle/2S10ELR8/276297]  |
| 专题 | 药物发现与设计中心 天然药物化学研究室 |
| 通讯作者 | Li, Bo |
| 作者单位 | 1.Univ Sci & Technol China, Nano Sci & Technol Inst, Suzhou 215123, Peoples R China 2.Shanghai Univ Tradit Chinese Med, Sch Pharm, Shanghai 201203, Peoples R China; 3.Chinese Acad Sci, Shanghai Inst Mat Med, CAS Key Lab Receptor Res, Shanghai 201203, Peoples R China; |
| 推荐引用方式 GB/T 7714 | Du, Guoxin,Li, Yisu,Ma, Shunan,et al. Efficient Determination of the Enantiomeric Purity and Absolute Configuration of Flavanones by Using (S)-3,3 '-Dibromo-1,1 '-bi-2-naphthol as a Chiral Solvating Agent[J]. JOURNAL OF NATURAL PRODUCTS,2015,78(12):2968-2974. |
| APA | Du, Guoxin.,Li, Yisu.,Ma, Shunan.,Wang, Rui.,Li, Bo.,...&Li, Yiming.(2015).Efficient Determination of the Enantiomeric Purity and Absolute Configuration of Flavanones by Using (S)-3,3 '-Dibromo-1,1 '-bi-2-naphthol as a Chiral Solvating Agent.JOURNAL OF NATURAL PRODUCTS,78(12),2968-2974. |
| MLA | Du, Guoxin,et al."Efficient Determination of the Enantiomeric Purity and Absolute Configuration of Flavanones by Using (S)-3,3 '-Dibromo-1,1 '-bi-2-naphthol as a Chiral Solvating Agent".JOURNAL OF NATURAL PRODUCTS 78.12(2015):2968-2974. |
入库方式： OAI收割
来源：上海药物研究所
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