Quantitative determination of ganoderic acid H in SunRecome by Reversed-phase high performance chromatography
文献类型：期刊论文
| 作者 | WANG Xiaoming2; GUAN Shuhong1 ; LIU Rongxia1; CHEN Guangtong2; BI Kaishun2; GUO Dean1
|
| 刊名 | Journal of Shenyang Pharmaceutical University
 |
| 出版日期 | 2007 |
| 卷号 | 24期号:7页码:407 |
| 关键词 | SunRecome (traditional Chinese medicines) ganoderic arid H RP-HPLC quantitative determination |
| ISSN号 | 1006-2858 |
| 其他题名 | RP-HPLC法测定双灵固本散中灵芝酸H的含量 |
| 文献子类 | Article |
| 英文摘要 | Objective To develop a RP-HPLC method for the quantitative determination of ganoderic acid H in the SunRecome(traditional Chinese medicines). Methods The chromatographic separation was achieved on an Agilent Zorbax SB-C_(18) column (250 mm * 4.6 mm, 5 mum) at 35℃, with a linear gradient of acetonitrile and 0.03% aqueous phosphoric acid(psi), at a flow rate of 1.0 mL·min~(-1). The detecting wavelength was set at 252 nm.Results The calibration curves showed good linearity(r < 0.999) within 16.34-408.5 kg·L~(-1). The average recovery of ganoderic acid H was 99.0% with RSD of 2.6% (n = 9). This method was successfully applied for analyzing 10 batches of SunRecome. The contents of ganoderic acid H were ranged from 0.130% to 0.348%. Conclusions The method is sensitive, accurate, reliable and suitable for the quality control of the SunRecome. |
| WOS研究方向 | Pharmacology & Pharmacy (provided by Clarivate Analytics) |
| 语种 | 中文 |
| CSCD记录号 | CSCD:2838341 |
| 源URL | [http://119.78.100.183/handle/2S10ELR8/268147]  |
| 专题 | 上海中药现代化研究中心 |
| 通讯作者 | GUO Dean |
| 作者单位 | 1.Shanghai Research Center for TCM Modernization, Shanghai Institute of Materia Medica, Shanghai Institutse for Biological Sciences, Shanghai 201203, China. 2.School of Pharmacy, Shenyang Pharmaceutical University, Shenyang, Liaoning 110016, China.; |
| 推荐引用方式 GB/T 7714 | WANG Xiaoming,GUAN Shuhong,LIU Rongxia,et al. Quantitative determination of ganoderic acid H in SunRecome by Reversed-phase high performance chromatography[J]. Journal of Shenyang Pharmaceutical University,2007,24(7):407. |
| APA | WANG Xiaoming,GUAN Shuhong,LIU Rongxia,CHEN Guangtong,BI Kaishun,&GUO Dean.(2007).Quantitative determination of ganoderic acid H in SunRecome by Reversed-phase high performance chromatography.Journal of Shenyang Pharmaceutical University,24(7),407. |
| MLA | WANG Xiaoming,et al."Quantitative determination of ganoderic acid H in SunRecome by Reversed-phase high performance chromatography".Journal of Shenyang Pharmaceutical University 24.7(2007):407. |
入库方式： OAI收割
来源：上海药物研究所
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