Identification of the major constituents in Shi-Quan-Da-Bu decoction by HPLC-ESI-MS/MS
文献类型：期刊论文
| 作者 | Tao, Sijia; Chen, Guangtong; Yang, Min; Deng, Shaosheng; Zhang, Jinqiang; Guo, De-an
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| 刊名 | NATURAL PRODUCT COMMUNICATIONS
 |
| 出版日期 | 2008 |
| 卷号 | 3期号:5页码:689-696 |
| 关键词 | traditional Chinese medicine Shi-Quan-Da-Bu decoction HPLC/DAD/MS |
| ISSN号 | 1934-578X |
| 文献子类 | Article |
| 英文摘要 | An HPLC/DAD/ESI/MS method was established for the qualitative analysis of the major constituents in Shi-Quan-Da-Bu decoction, a traditional Chinese medicinal formula. Based on the chromatographic separation of most of the constituents of Shi-Quan-Da-Bu decoction on a Zorbax SB-C-18 column with water-acetonitrile as the mobile phase, more than 150 components were detected by LC-MS. Among them, 36 major components, including flavonoids, triterpenoid saponins, iridoid glycosides, phathalides and phenylpropionic acids were either identified or tentatively characterized. Twenty one compounds were identified by ESI-MS and comparison of their retention times with those of reference standards. The other 15 compounds were deduced according to their MS and UV spectra and retention behaviors by comparing the results with those reported in the literature. Most of these compounds were derived mainly from Paeonia lactiflora, Glycyrrhiza uralensis, Panax ginseng, Ligusticum chuanxiong, Angelica sinensis and Astragalus membranaceus. |
| WOS关键词 | IONIZATION MASS-SPECTROMETRY ; PERFORMANCE LIQUID-CHROMATOGRAPHY ; JUZEN-TAIHO-TO ; PRESSURE CHEMICAL-IONIZATION ; PHENOLIC-COMPOUNDS ; ENDOMETRIAL CARCINOGENESIS ; ASTRAGALUS-MONGHOLICUS ; GLYCYRRHIZA-URALENSIS ; QUANTITATIVE-ANALYSES ; SALVIA-MILTIORRHIZA |
| WOS研究方向 | Pharmacology & Pharmacy ; Food Science & Technology |
| 语种 | 英语 |
| WOS记录号 | WOS:000256280100007 |
| 出版者 | NATURAL PRODUCTS INC |
| 源URL | [http://119.78.100.183/handle/2S10ELR8/273070]  |
| 专题 | 上海中药现代化研究中心 |
| 通讯作者 | Guo, De-an |
| 作者单位 | Chinese Acad Sci, Shanghai Inst Biol Sci, Shanghai Inst Mat Med, Shanghai Res Ctr Modernizat Tradit Chinese Med, Shanghai 201203, Peoples R China |
| 推荐引用方式 GB/T 7714 | Tao, Sijia,Chen, Guangtong,Yang, Min,et al. Identification of the major constituents in Shi-Quan-Da-Bu decoction by HPLC-ESI-MS/MS[J]. NATURAL PRODUCT COMMUNICATIONS,2008,3(5):689-696. |
| APA | Tao, Sijia,Chen, Guangtong,Yang, Min,Deng, Shaosheng,Zhang, Jinqiang,&Guo, De-an.(2008).Identification of the major constituents in Shi-Quan-Da-Bu decoction by HPLC-ESI-MS/MS.NATURAL PRODUCT COMMUNICATIONS,3(5),689-696. |
| MLA | Tao, Sijia,et al."Identification of the major constituents in Shi-Quan-Da-Bu decoction by HPLC-ESI-MS/MS".NATURAL PRODUCT COMMUNICATIONS 3.5(2008):689-696. |
入库方式： OAI收割
来源：上海药物研究所
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