Detection, characterization and identification of phenolic acids in Danshen using high-performance. liquid chromatography with diode array detection and electrospray ionization mass spectrometry
文献类型:期刊论文
作者 | Liu, Ai-Hua; Guo, Hui; Ye, Min; Lin, Yan-Hua; Sun, Hang-Hao; Xu, Man; Guo, De-An![]() |
刊名 | JOURNAL OF CHROMATOGRAPHY A
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出版日期 | 2007-08-17 |
卷号 | 1161期号:1-2页码:170-182 |
关键词 | phenolic acid salvia miltiorrhiza HPLC-DAD-ESI-MSn |
ISSN号 | 0021-9673 |
DOI | 10.1016/j.chroma.2007.05.081 |
文献子类 | Article |
英文摘要 | By using HPLC-diode array detection-electrospray ion trap tandem mass spectrometry (HPLC-DAD-ESI-MSn) in negative ion mode, we have analyzed the fragmentation pathways of 11 phenolic acids which were isolated from Danshen. Then the extract of Danshen was analyzed, and a total of 42 phenolic acids, including sixteen new minor constituents, were identified or tentatively identified for the first time. A new solidphase extraction (SPE) method, new HPLC separation method, new liquid chromatography (LC)-MS and LC-MSn (n = 3-5) data and proposed fragmentation pathways, LC retention time for phenolic acids are reported. (c) 2007 Elsevier B.V. All rights reserved. |
WOS关键词 | CHINESE MEDICINAL PREPARATIONS ; SALVIA-MILTIORRHIZA ; HPLC-DAD ; ROOTS ; QUANTIFICATION ; YUNNANENSIS ; METABOLITES ; TANSHINONES ; DEPSIDE |
WOS研究方向 | Biochemistry & Molecular Biology ; Chemistry |
语种 | 英语 |
WOS记录号 | WOS:000248891500023 |
出版者 | ELSEVIER SCIENCE BV |
源URL | [http://119.78.100.183/handle/2S10ELR8/273173] ![]() |
专题 | 上海中药现代化研究中心 |
通讯作者 | Guo, De-An |
作者单位 | 1.Peking Univ, Sch Pharmaceut Sci, State Key Lab Nat & Biomimet Drugs, Beijing 100083, Peoples R China 2.Chinese Acad Sci, Shanghai Inst Biol Sci, Shanghai Inst Mat Med, Shanghai Res Ctr TCM Modernizat, Shanghai 201203, Peoples R China |
推荐引用方式 GB/T 7714 | Liu, Ai-Hua,Guo, Hui,Ye, Min,et al. Detection, characterization and identification of phenolic acids in Danshen using high-performance. liquid chromatography with diode array detection and electrospray ionization mass spectrometry[J]. JOURNAL OF CHROMATOGRAPHY A,2007,1161(1-2):170-182. |
APA | Liu, Ai-Hua.,Guo, Hui.,Ye, Min.,Lin, Yan-Hua.,Sun, Hang-Hao.,...&Guo, De-An.(2007).Detection, characterization and identification of phenolic acids in Danshen using high-performance. liquid chromatography with diode array detection and electrospray ionization mass spectrometry.JOURNAL OF CHROMATOGRAPHY A,1161(1-2),170-182. |
MLA | Liu, Ai-Hua,et al."Detection, characterization and identification of phenolic acids in Danshen using high-performance. liquid chromatography with diode array detection and electrospray ionization mass spectrometry".JOURNAL OF CHROMATOGRAPHY A 1161.1-2(2007):170-182. |
入库方式: OAI收割
来源:上海药物研究所
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