QUALITY ASSESSMENT FOR PORTULACA OLERACEA BY MULTI-COMPONENT QUANTIFICATION, CHROMATOGRAPHIC FINGERPRINT AND RELATED CHEMOMETRIC ANALYSIS
文献类型：期刊论文
| 作者 | Lin, Yun1,2; Li, Zhixiong2 ; Wu, Bin2; Yang, Quanjun2; Jiang, Jian1; Huang, Chenggang2
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| 刊名 | JOURNAL OF LIQUID CHROMATOGRAPHY & RELATED TECHNOLOGIES
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| 出版日期 | 2012 |
| 卷号 | 35期号:19页码:2655-2668 |
| 关键词 | chromatographic fingerprint hierarchical cluster analysis multi-component quantification Portulaca oleracea principal component analysis ultra performance liquid chromatography |
| ISSN号 | 1082-6076 |
| DOI | 10.1080/10826076.2011.637268 |
| 文献子类 | Article |
| 英文摘要 | For the reliable quality control of Portulaca oleracea L., multi-component simultaneous quantification, chromatographic fingerprint, and related chemometric techniques were applied for exploration. In order to obtain the best extraction efficiency and chromatographic resolution, extraction method and chromatographic conditions were optimized. The samples from different origins were collected and identified. With the use of the Ultra Performance Liquid Chromatography (UPLC) and coupled Photo-Diode Array (PDA) detector, 18 characteristic peaks were comprised in the fingerprint common pattern. Among them, four marked components, including hesperidin, kaempferol, lupeol, and myricetin, were quantified. Similarity evaluation, principal component analysis, and hierachical cluster analysis were applied to demonstrate the distinction. All the results implied two conclusions: (1) chemical compositions of P. oleracea from different origins were very different; and (2) the simple, feasible, and effective method for quality control of P. oleracea was to determine the content of lupeol and then make a comparison of fingerprint atlas. |
| WOS关键词 | HPLC |
| 资助项目 | National Science & Technology Major Project "Key New Drug Creation and Manufacturing Program," China[2009ZX09301-001] ; National Science & Technology Major Project "Key New Drug Creation and Manufacturing Program," China[2009ZX09308-005] ; Science and Technology Commission of Shanghai Municipality[09DZ1971200] |
| WOS研究方向 | Biochemistry & Molecular Biology ; Chemistry |
| 语种 | 英语 |
| WOS记录号 | WOS:000315210800001 |
| 出版者 | TAYLOR & FRANCIS INC |
| 源URL | [http://119.78.100.183/handle/2S10ELR8/278227]  |
| 专题 | 上海中药现代化研究中心 |
| 通讯作者 | Jiang, Jian |
| 作者单位 | 1.Shanghai Univ Tradit Chinese Med, Shuguang Hosp, Dept Clin Pharmacol, Shanghai 201203, Peoples R China; 2.Chinese Acad Sci, Shanghai Inst Mat Med, Shanghai Inst Biol Sci, Shanghai 201203, Peoples R China |
| 推荐引用方式 GB/T 7714 | Lin, Yun,Li, Zhixiong,Wu, Bin,et al. QUALITY ASSESSMENT FOR PORTULACA OLERACEA BY MULTI-COMPONENT QUANTIFICATION, CHROMATOGRAPHIC FINGERPRINT AND RELATED CHEMOMETRIC ANALYSIS[J]. JOURNAL OF LIQUID CHROMATOGRAPHY & RELATED TECHNOLOGIES,2012,35(19):2655-2668. |
| APA | Lin, Yun,Li, Zhixiong,Wu, Bin,Yang, Quanjun,Jiang, Jian,&Huang, Chenggang.(2012).QUALITY ASSESSMENT FOR PORTULACA OLERACEA BY MULTI-COMPONENT QUANTIFICATION, CHROMATOGRAPHIC FINGERPRINT AND RELATED CHEMOMETRIC ANALYSIS.JOURNAL OF LIQUID CHROMATOGRAPHY & RELATED TECHNOLOGIES,35(19),2655-2668. |
| MLA | Lin, Yun,et al."QUALITY ASSESSMENT FOR PORTULACA OLERACEA BY MULTI-COMPONENT QUANTIFICATION, CHROMATOGRAPHIC FINGERPRINT AND RELATED CHEMOMETRIC ANALYSIS".JOURNAL OF LIQUID CHROMATOGRAPHY & RELATED TECHNOLOGIES 35.19(2012):2655-2668. |
入库方式： OAI收割
来源：上海药物研究所
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