PPh3/I-2/HCOOH: An efficient CO source for the synthesis of phthalimides
文献类型：期刊论文
| 作者 | Wang, Yingying1,2; Zhou, Yang1,2; Lei, Min1,2 ; Hou, Jinjun1,2; Jin, Qinghao1,2; Guo, Dean1,2; Wu, Wanying1,2
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| 刊名 | TETRAHEDRON
 |
| 出版日期 | 2019-03-01 |
| 卷号 | 75期号:9页码:1180-1185 |
| 关键词 | Phthalimide PPh3/I-2/HCOOH 2-lodobenzamide Pd(OAc)(2) CO source |
| ISSN号 | 0040-4020 |
| DOI | 10.1016/j.tet.2019.01.023 |
| 通讯作者 | Lei, Min(mlei@simm.ac.cn) ; Wu, Wanying(wanyingwu@simm.ac.cn) |
| 英文摘要 | A straightforward and general method has been developed for the synthesis of phthalimide derivatives from 2-iodobenzamides and PPh3/I-2/HCOOH in the presence of a catalytic amount of Pd(OAc)(2). The reaction results demonstrate that PPh3/I-2/HCOOH is a facile, efficient and safe CO source. The whole process is carried out in toluene at 80 degrees C and furnishes the desired products in good to excellent yields. (C) 2019 Published by Elsevier Ltd. |
| WOS关键词 | PALLADIUM-CATALYZED SYNTHESIS ; REDUCTIVE CARBONYLATION ; DIRECT FORMYLATION ; AROMATIC IODIDES ; ARYL IODIDES ; ALDEHYDES ; ACID ; NITROGEN |
| 资助项目 | Special Fund for Strategic Pilot Technology Chinese Academy of Sciences[XDA12020379] |
| WOS研究方向 | Chemistry |
| 语种 | 英语 |
| WOS记录号 | WOS:000459522800009 |
| 出版者 | PERGAMON-ELSEVIER SCIENCE LTD |
| 源URL | [http://119.78.100.183/handle/2S10ELR8/290462]  |
| 专题 | 中国科学院上海药物研究所 |
| 通讯作者 | Lei, Min; Wu, Wanying |
| 作者单位 | 1.Univ Chinese Acad Sci, Beijing 100049, Peoples R China 2.Chinese Acad Sci, Shanghai Res Ctr Modernizat Tradit Chinese Med, Natl Engn Lab TCM Standardizat Technol, Shanghai Inst Mat Med, Shanghai 201203, Peoples R China |
| 推荐引用方式 GB/T 7714 | Wang, Yingying,Zhou, Yang,Lei, Min,et al. PPh3/I-2/HCOOH: An efficient CO source for the synthesis of phthalimides[J]. TETRAHEDRON,2019,75(9):1180-1185. |
| APA | Wang, Yingying.,Zhou, Yang.,Lei, Min.,Hou, Jinjun.,Jin, Qinghao.,...&Wu, Wanying.(2019).PPh3/I-2/HCOOH: An efficient CO source for the synthesis of phthalimides.TETRAHEDRON,75(9),1180-1185. |
| MLA | Wang, Yingying,et al."PPh3/I-2/HCOOH: An efficient CO source for the synthesis of phthalimides".TETRAHEDRON 75.9(2019):1180-1185. |
入库方式： OAI收割
来源：上海药物研究所
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