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Pressure-Assisted Method for the Preparations of High-Quality AaGaS(2) and AgGaGeS4 Crystals for Mid-Infrared Laser Applications

文献类型：期刊论文

作者Huang, Changbao; Mao, Mingsheng; Wu, Haixin; Ma, Jiaren
刊名INORGANIC CHEMISTRY
出版日期2018-12-03
卷号57期号:23页码:14866-14871
ISSN号0020-1669
DOI10.1021/acs.inorgchem.8b02626
通讯作者Wu, Haixin(hxwu@aiofm.ac.cn)
英文摘要Recently developed chalcogenides nonlinear optical crystals have potential application in mid- to far infrared laser fields. However, high-quality single crystals are hard to be prepared because of high vapor pressure of sulfur component and decomposition of chalcogenides during the polycrystalline synthesis and single-crystal growth. A pressure assisted technique was performed to prepare stoichiometric AgGaS2 and AgGaGeS4 polycrystalline materials. On the basis of the synthesized polycrystalline materials, high-quality AgGaS2 and AgGaGeS4 single crystals were successfully obtained using the seed directional Bridgman method with a well-designed crucible-capsule technique. These single crystals possess high homogeneity and low absorption coefficient, making it can be applied in nonlinear optical experiments. The pressure-assisted method can also be suitable to prepare other chalcogenide and phosphide compounds. The method of polycrystalline synthesis and single crystals growth described in this work will be helpful for preparing other chalcogenides nonlinear optical crystals.
WOS关键词NONLINEAR-OPTICAL MATERIALS ; PHASE-MATCHING PROPERTIES ; DAMAGE THRESHOLD ; SINGLE-CRYSTALS ; BAND-GAP ; GROWTH ; GENERATION ; PARAMETERS ; CONVERSION ; SN
资助项目National Natural Science Foundation of China (NSFC)[51702323]
WOS研究方向Chemistry
语种英语
出版者AMER CHEMICAL SOC
WOS记录号WOS:000452344400046
资助机构National Natural Science Foundation of China (NSFC) ; National Natural Science Foundation of China (NSFC) ; National Natural Science Foundation of China (NSFC) ; National Natural Science Foundation of China (NSFC) ; National Natural Science Foundation of China (NSFC) ; National Natural Science Foundation of China (NSFC) ; National Natural Science Foundation of China (NSFC) ; National Natural Science Foundation of China (NSFC) ; National Natural Science Foundation of China (NSFC) ; National Natural Science Foundation of China (NSFC) ; National Natural Science Foundation of China (NSFC) ; National Natural Science Foundation of China (NSFC) ; National Natural Science Foundation of China (NSFC) ; National Natural Science Foundation of China (NSFC) ; National Natural Science Foundation of China (NSFC) ; National Natural Science Foundation of China (NSFC)
源URL[http://ir.hfcas.ac.cn:8080/handle/334002/40611]  
专题合肥物质科学研究院_中科院安徽光学精密机械研究所
通讯作者Wu, Haixin
作者单位Chinese Acad Sci, Anhui Inst Opt & Fine Mech, Anhui Prov Key Lab Photon Devices & Mat, Hefei 230031, Anhui, Peoples R China
推荐引用方式
GB/T 7714		 Huang, Changbao,Mao, Mingsheng,Wu, Haixin,et al. Pressure-Assisted Method for the Preparations of High-Quality AaGaS(2) and AgGaGeS4 Crystals for Mid-Infrared Laser Applications[J]. INORGANIC CHEMISTRY,2018,57(23):14866-14871.
APA Huang, Changbao,Mao, Mingsheng,Wu, Haixin,&Ma, Jiaren.(2018).Pressure-Assisted Method for the Preparations of High-Quality AaGaS(2) and AgGaGeS4 Crystals for Mid-Infrared Laser Applications.INORGANIC CHEMISTRY,57(23),14866-14871.
MLA Huang, Changbao,et al."Pressure-Assisted Method for the Preparations of High-Quality AaGaS(2) and AgGaGeS4 Crystals for Mid-Infrared Laser Applications".INORGANIC CHEMISTRY 57.23(2018):14866-14871.

入库方式： OAI收割

来源：合肥物质科学研究院

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