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  2. 地质与地球物理研究所
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  4. 岩石圈演化国家重点实验室
Comparative Study of Three Mixing Methods in Fusion Technique for Determining Major and Minor Elements Using Wavelength Dispersive X-ray Fluorescence Spectroscopy

文献类型：期刊论文

作者Zhang, Dan-Ping1,2,3; Xue, Ding-Shuai1; Liu, Yan-Hong1; Wan, Bo1; Guo, Qian1; Guo, Ju-Jie1
刊名SENSORS
出版日期2020-09-01
卷号20期号:18页码:17
关键词wavelength dispersive X-ray fluorescence spectroscopy sample preparation procedure fused glass disc shaker cup method
DOI10.3390/s20185325
英文摘要Accurate analysis using a simple and rapid procedure is always the most important pursuit of analytical chemists. In this study, a new sample preparation procedure, namely the shaker cup (SH) method, was designed and compared with two sample preparation procedures, commonly used in the laboratory, from three aspects: homogeneity of the sample-flux mixture, potential for sample contamination, and sample preparation time. For the three methods, a set of 54 certified reference materials (CRMs) was used to establish the calibration curves, while another set of 19 CRMs was measured to validate the results. In the calibration procedures, the matrix effects were corrected using the theoretical alpha coefficient method combined with the experimental coefficient method. The data of the major oxides (SiO2, TiO2, Al2O3, TFe2O3, MnO, MgO, CaO, Na2O, K2O, and P2O5) and minor elements (Cr, Cu, Ba, Ni, Sr, V, Zr, and Zn) obtained by wavelength dispersive X-ray fluorescence spectroscopy (WD-XRF) were compared using two derivative equations based on the findings by Laurence Whitty-Leveille. The results revealed that the WD-XRF measured values using the SH method best agreed with the values recommended in the literature.
WOS关键词GEOLOGICAL SAMPLES ; SILICATE ROCKS ; GLASS BEAD ; XRF ; GEOCHEMISTRY ; VOLCANISM ; INSIGHTS ; BOUNDARY ; PACIFIC ; ORIGIN
资助项目National Key R&D Program of China[2019YFA0708400] ; Experimental Technology Innovation Fund of the Institute of Geology and Geophysics, Chinese Academy of Sciences[T202001] ; Equipment function development technology innovation projects of China science academy[IGG201702] ; National Natural Science Foundation of China[41403021] ; National Natural Science Foundation of China[41703021] ; National Natural Science Foundation of China[41525012] ; Open Research Foundation of the Key Laboratory of Mineral Resources, Institute of Geology and Geophysics, Chinese Academy of Sciences[12]
WOS研究方向Chemistry ; Engineering ; Instruments & Instrumentation
语种英语
WOS记录号WOS:000580127700001
出版者MDPI
资助机构National Key R&D Program of China ; National Key R&D Program of China ; National Key R&D Program of China ; National Key R&D Program of China ; Experimental Technology Innovation Fund of the Institute of Geology and Geophysics, Chinese Academy of Sciences ; Experimental Technology Innovation Fund of the Institute of Geology and Geophysics, Chinese Academy of Sciences ; Experimental Technology Innovation Fund of the Institute of Geology and Geophysics, Chinese Academy of Sciences ; Experimental Technology Innovation Fund of the Institute of Geology and Geophysics, Chinese Academy of Sciences ; Equipment function development technology innovation projects of China science academy ; Equipment function development technology innovation projects of China science academy ; Equipment function development technology innovation projects of China science academy ; Equipment function development technology innovation projects of China science academy ; National Natural Science Foundation of China ; National Natural Science Foundation of China ; National Natural Science Foundation of China ; National Natural Science Foundation of China ; Open Research Foundation of the Key Laboratory of Mineral Resources, Institute of Geology and Geophysics, Chinese Academy of Sciences ; Open Research Foundation of the Key Laboratory of Mineral Resources, Institute of Geology and Geophysics, Chinese Academy of Sciences ; Open Research Foundation of the Key Laboratory of Mineral Resources, Institute of Geology and Geophysics, Chinese Academy of Sciences ; Open Research Foundation of the Key Laboratory of Mineral Resources, Institute of Geology and Geophysics, Chinese Academy of Sciences ; National Key R&D Program of China ; National Key R&D Program of China ; National Key R&D Program of China ; National Key R&D Program of China ; Experimental Technology Innovation Fund of the Institute of Geology and Geophysics, Chinese Academy of Sciences ; Experimental Technology Innovation Fund of the Institute of Geology and Geophysics, Chinese Academy of Sciences ; Experimental Technology Innovation Fund of the Institute of Geology and Geophysics, Chinese Academy of Sciences ; Experimental Technology Innovation Fund of the Institute of Geology and Geophysics, Chinese Academy of Sciences ; Equipment function development technology innovation projects of China science academy ; Equipment function development technology innovation projects of China science academy ; Equipment function development technology innovation projects of China science academy ; Equipment function development technology innovation projects of China science academy ; National Natural Science Foundation of China ; National Natural Science Foundation of China ; National Natural Science Foundation of China ; National Natural Science Foundation of China ; Open Research Foundation of the Key Laboratory of Mineral Resources, Institute of Geology and Geophysics, Chinese Academy of Sciences ; Open Research Foundation of the Key Laboratory of Mineral Resources, Institute of Geology and Geophysics, Chinese Academy of Sciences ; Open Research Foundation of the Key Laboratory of Mineral Resources, Institute of Geology and Geophysics, Chinese Academy of Sciences ; Open Research Foundation of the Key Laboratory of Mineral Resources, Institute of Geology and Geophysics, Chinese Academy of Sciences ; National Key R&D Program of China ; National Key R&D Program of China ; National Key R&D Program of China ; National Key R&D Program of China ; Experimental Technology Innovation Fund of the Institute of Geology and Geophysics, Chinese Academy of Sciences ; Experimental Technology Innovation Fund of the Institute of Geology and Geophysics, Chinese Academy of Sciences ; Experimental Technology Innovation Fund of the Institute of Geology and Geophysics, Chinese Academy of Sciences ; Experimental Technology Innovation Fund of the Institute of Geology and Geophysics, Chinese Academy of Sciences ; Equipment function development technology innovation projects of China science academy ; Equipment function development technology innovation projects of China science academy ; Equipment function development technology innovation projects of China science academy ; Equipment function development technology innovation projects of China science academy ; National Natural Science Foundation of China ; National Natural Science Foundation of China ; National Natural Science Foundation of China ; National Natural Science Foundation of China ; Open Research Foundation of the Key Laboratory of Mineral Resources, Institute of Geology and Geophysics, Chinese Academy of Sciences ; Open Research Foundation of the Key Laboratory of Mineral Resources, Institute of Geology and Geophysics, Chinese Academy of Sciences ; Open Research Foundation of the Key Laboratory of Mineral Resources, Institute of Geology and Geophysics, Chinese Academy of Sciences ; Open Research Foundation of the Key Laboratory of Mineral Resources, Institute of Geology and Geophysics, Chinese Academy of Sciences ; National Key R&D Program of China ; National Key R&D Program of China ; National Key R&D Program of China ; National Key R&D Program of China ; Experimental Technology Innovation Fund of the Institute of Geology and Geophysics, Chinese Academy of Sciences ; Experimental Technology Innovation Fund of the Institute of Geology and Geophysics, Chinese Academy of Sciences ; Experimental Technology Innovation Fund of the Institute of Geology and Geophysics, Chinese Academy of Sciences ; Experimental Technology Innovation Fund of the Institute of Geology and Geophysics, Chinese Academy of Sciences ; Equipment function development technology innovation projects of China science academy ; Equipment function development technology innovation projects of China science academy ; Equipment function development technology innovation projects of China science academy ; Equipment function development technology innovation projects of China science academy ; National Natural Science Foundation of China ; National Natural Science Foundation of China ; National Natural Science Foundation of China ; National Natural Science Foundation of China ; Open Research Foundation of the Key Laboratory of Mineral Resources, Institute of Geology and Geophysics, Chinese Academy of Sciences ; Open Research Foundation of the Key Laboratory of Mineral Resources, Institute of Geology and Geophysics, Chinese Academy of Sciences ; Open Research Foundation of the Key Laboratory of Mineral Resources, Institute of Geology and Geophysics, Chinese Academy of Sciences ; Open Research Foundation of the Key Laboratory of Mineral Resources, Institute of Geology and Geophysics, Chinese Academy of Sciences
源URL[http://ir.iggcas.ac.cn/handle/132A11/98307]  
专题地质与地球物理研究所_岩石圈演化国家重点实验室
通讯作者Xue, Ding-Shuai
作者单位1.Chinese Acad Sci, Inst Geol & Geophys, Beijing 100029, Peoples R China
2.Chinese Acad Sci, Innovat Acad Earth Sci, Beijing 100029, Peoples R China
3.Chinese Acad Sci, Inst Geol & Geophys, State Key Lab Lithospher Evolut, Beijing 100029, Peoples R China
推荐引用方式
GB/T 7714		 Zhang, Dan-Ping,Xue, Ding-Shuai,Liu, Yan-Hong,et al. Comparative Study of Three Mixing Methods in Fusion Technique for Determining Major and Minor Elements Using Wavelength Dispersive X-ray Fluorescence Spectroscopy[J]. SENSORS,2020,20(18):17.
APA Zhang, Dan-Ping,Xue, Ding-Shuai,Liu, Yan-Hong,Wan, Bo,Guo, Qian,&Guo, Ju-Jie.(2020).Comparative Study of Three Mixing Methods in Fusion Technique for Determining Major and Minor Elements Using Wavelength Dispersive X-ray Fluorescence Spectroscopy.SENSORS,20(18),17.
MLA Zhang, Dan-Ping,et al."Comparative Study of Three Mixing Methods in Fusion Technique for Determining Major and Minor Elements Using Wavelength Dispersive X-ray Fluorescence Spectroscopy".SENSORS 20.18(2020):17.

入库方式： OAI收割

来源：地质与地球物理研究所

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