Optimization of Vortex-Assisted Dispersive Liquid-Liquid Microextraction for the Simultaneous Quantitation of Eleven Non-Anthocyanin Polyphenols in Commercial Blueberry Using the Multi-Objective Response Surface Methodology and Desirability Function Approach
文献类型：期刊论文
| 作者 | Xue, Ying1,2,3; Xu, Xian-Shun2; Yong, Li2; Hu, Bin2; Li, Xing-De1; Zhong, Shi-Hong3; Li, Yi3; Xie, Jing3; Qing, Lin-Sen1,3 |
| 刊名 | MOLECULES
 |
| 出版日期 | 2018-11-01 |
| 卷号 | 23期号:11页码:2921 |
| 关键词 | blueberry non-anthocyanin polyphenol vortex-assisted dispersive liquid-liquid microextraction response surface methodology desirability function approach |
| ISSN号 | 1420-3049 |
| DOI | 10.3390/molecules23112921 |
| 产权排序 | 2 |
| 文献子类 | Article |
| 英文摘要 | In the present study, 11 non-anthocyanin polyphenols, gallic acid, protocatechuate, vanillic acid, syringic acid, ferulic acid, quercetin, catechin, epicatechin, epigallocatechin gallate, gallocatechin gallate and epicatechin gallatewere firstly screened and identified from blueberries using an ultra performance liquid chromatography-time of flight mass spectrography (UPLC-TOF/MS) method. Then, a sample preparation method was developed based on vortex-assisted dispersive liquid-liquid microextraction. The microextraction conditions, including the amount of ethyl acetate, the amount of acetonitrile and the solution pH, were optimized through the multi-objective response surface methodology and desirability function approach. Finally, an ultra performance liquid chromatography-triple quadrupole mass spectrography (UPLC-QqQ/MS) method was developed to determine the 11 non-anthocyanin polyphenols in 25 commercial blueberry samples from Sichuan province and Chongqing city. The results show that this new method with high accuracy, good precision and simple operation characteristics, can be used to determine non-anthocyanin polyphenols in blueberries and is expected to be used in the analysis of other fruits and vegetables. |
| 学科主题 | Chemistry |
| URL标识 | 查看原文 |
| WOS关键词 | PHENOLIC-ACIDS ; EXTRACTION ; HPLC ; FRUIT ; IDENTIFICATION ; CHROMATOGRAPHY ; ANTIOXIDANT ; COMBINATION ; ULTRASOUND ; SEPARATION |
| WOS研究方向 | Biochemistry & Molecular Biology ; Chemistry |
| 语种 | 英语 |
| WOS记录号 | WOS:000451641900193 |
| 出版者 | MDPI |
| 源URL | [http://210.75.237.14/handle/351003/30119]  |
| 专题 | 国家天然药物工程技术研究中心_天然产物研究 |
| 作者单位 | 1.Chinese Acad Sci, Chengdu Inst Biol, Chengdu 610041, Sichuan, Peoples R China; 2.Sichuan Prov Ctr Dis Control & Prevent, Chengdu 610041, Sichuan, Peoples R China 3.Chengdu Med Coll, Sch Pharm, Collaborat Innovat Ctr Sichuan Elderly Care & Hlt, Chengdu 610500, Peoples R China; |
| 推荐引用方式 GB/T 7714 | Xue, Ying,Xu, Xian-Shun,Yong, Li,et al. Optimization of Vortex-Assisted Dispersive Liquid-Liquid Microextraction for the Simultaneous Quantitation of Eleven Non-Anthocyanin Polyphenols in Commercial Blueberry Using the Multi-Objective Response Surface Methodology and Desirability Function Approach[J]. MOLECULES,2018,23(11):2921. |
| APA | Xue, Ying.,Xu, Xian-Shun.,Yong, Li.,Hu, Bin.,Li, Xing-De.,...&Qing, Lin-Sen.(2018).Optimization of Vortex-Assisted Dispersive Liquid-Liquid Microextraction for the Simultaneous Quantitation of Eleven Non-Anthocyanin Polyphenols in Commercial Blueberry Using the Multi-Objective Response Surface Methodology and Desirability Function Approach.MOLECULES,23(11),2921. |
| MLA | Xue, Ying,et al."Optimization of Vortex-Assisted Dispersive Liquid-Liquid Microextraction for the Simultaneous Quantitation of Eleven Non-Anthocyanin Polyphenols in Commercial Blueberry Using the Multi-Objective Response Surface Methodology and Desirability Function Approach".MOLECULES 23.11(2018):2921. |
入库方式： OAI收割
来源：成都生物研究所
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