Tailoring of pyramid cobalt doped nickel oxide nanostructures by composite-hydroxide-mediated approach
文献类型:期刊论文
作者 | Zeb, Aurang; Arfan, Muhammad; Shahid, Tauseef; Bin Masood, Taha; Wattoo, Abdul Ghafar; Song, Zhenlun; Shahzad, Moazzam; Ansari, Shehzad Munir |
刊名 | MATERIALS CHEMISTRY AND PHYSICS
![]() |
出版日期 | 2020 |
卷号 | 239 |
关键词 | GAS-SENSING PROPERTIES NANOCRYSTALLINE NIO FACILE SYNTHESIS NANOPARTICLES MICROSPHERES NANOSHEETS |
DOI | 10.1016/j.matchemphys.2019.122036 |
英文摘要 | Nickel oxide nanostructures have been synthesized successfully by composite hydroxide mediated (CHM) approach at 200 degrees C for various cobalt concentrations (0%, 5%, 10% and 15%). Incorporation of cobalt was explored by employing X-ray diffraction (XRD), Fourier transform infrared spectroscopy (PTIR), scanning electron microscopy (SEM, and ultraviolet visible spectroscopy. An influence of increase in cobalt doping on average crystallite size was found from 31 to 56 nm. The Increase in crystallite size is due to the introduction of point defects and oxygen vacancies caused by the incorporation of Co ions in NiO lattice. The influence of defects is also seen from variation in lattice parameters and X-ray density. The effect of incorporation of increasing cobalt contents was seen from SEM micrographs. The spherical characteristics of pure NiO nanostructures changed to sharp edge pyramids with smooth surfaces. The growth of pyramids is evident with increase in side length 421-691 rim for various cobalt concentrations (5%, 10% and 15%). FT-IR confirms the purity of product while the band gap was estimated by UV-Vis spectroscopy which was found from 5.59 to 1.50 eV. |
学科主题 | Materials Science |
源URL | [http://ir.nimte.ac.cn/handle/174433/20269] ![]() |
专题 | 2020专题 2020专题_期刊论文 |
作者单位 | Shahid, T (corresponding author), Chinese Acad Sci, Ningbo Inst Mat Technol & Engn, Zhejiang Prov Key Lab Magnet Mat & Applicat Techn, CAS Key Lab Magnet Mat & Devices, Ningbo 315201, Zhejiang, Peoples R China. |
推荐引用方式 GB/T 7714 | Zeb, Aurang,Arfan, Muhammad,Shahid, Tauseef,et al. Tailoring of pyramid cobalt doped nickel oxide nanostructures by composite-hydroxide-mediated approach[J]. MATERIALS CHEMISTRY AND PHYSICS,2020,239. |
APA | Zeb, Aurang.,Arfan, Muhammad.,Shahid, Tauseef.,Bin Masood, Taha.,Wattoo, Abdul Ghafar.,...&Ansari, Shehzad Munir.(2020).Tailoring of pyramid cobalt doped nickel oxide nanostructures by composite-hydroxide-mediated approach.MATERIALS CHEMISTRY AND PHYSICS,239. |
MLA | Zeb, Aurang,et al."Tailoring of pyramid cobalt doped nickel oxide nanostructures by composite-hydroxide-mediated approach".MATERIALS CHEMISTRY AND PHYSICS 239(2020). |
入库方式: OAI收割
来源:宁波材料技术与工程研究所
浏览0
下载0
收藏0
其他版本
除非特别说明,本系统中所有内容都受版权保护,并保留所有权利。