Silver nanoparticles synthesized using Allium ampeloprasum L. leaf extract: Characterization and performance in catalytic reduction of 4-nitrophenol and antioxidant activity
文献类型:期刊论文
作者 | Khoshnamvand, Mehdi; Huo, Can; Liu, Jingfu |
刊名 | JOURNAL OF MOLECULAR STRUCTURE
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出版日期 | 2019-01-05 |
卷号 | 1175页码:90-96 |
关键词 | Silver nanoparticles Allium ampeloprasum Leaf extract Characterization |
ISSN号 | 0022-2860 |
英文摘要 | A green approach for biosynthesis of silver nanoparticles (AgNPs) is developed using A. ampeloprasum leaf extract. The as-synthesized nanoparticles were characterized by UV visible, transmission electron microscopy (TEM), scanning electron microscopy (SEM), energy-dispersive X-ray spectroscopy (EDX), Xray diffraction (XRD), fourier transform infrared spectroscopy (FTIR) and zeta sizer (ZS). The formation of AgNPs was confirmed by changing the colour of solution from colourless to light brown and the presence of absorption peaks between 420 and 440 nm using UV spectra. The TEM analysis of AgNPs showed the particle sizes ranged between 2 and 43 nm, with shapes of quasi-spherical, spherical, ellipsoidal, hexagonal and irregular. The crystalline and face centered cubic (FCC) structure of AgNPs was obtained by XRD study. In addition, the FTIR spectrum of AgNPs showed the presence of different functional groups that may be associated with the reduction of Ag ions to AgNPs. The yield of AgNPs was determined around 99.95% by ICP-MS quantification after centrifugal ultrafiltration. The biosynthesized AgNPs exhibited catalytic activity in the reduction of the toxic organic pollutant of 4-nitrophenol to 4-aminophenol, and antioxidant activity against DPPH center dot (2,2-diphenyl-1-picrylhydrzyl) and ABTS(+center dot) (2,2'azino-bis (3-ethylbenzothiazoline-6-sulphonic acid)) radicals. This approach does not require any toxic substance, is quite cheap and readily to be performed in a single pot process. (C) 2018 Elsevier B.V. All rights reserved. |
源URL | [http://ir.rcees.ac.cn/handle/311016/43013] ![]() |
专题 | 生态环境研究中心_环境化学与生态毒理学国家重点实验室 |
作者单位 | 1.North China Elect Power Univ, Sch Environm Sci & Engn, Baoding 071000, Peoples R China 2.Univ Chinese Acad Sci, Beijing 100049, Peoples R China 3.Chinese Acad Sci, Res Ctr Ecoenvironm Sci, State Key Lab Environm Chem & Ecotoxicol, POB 2871, Beijing 100085, Peoples R China |
推荐引用方式 GB/T 7714 | Khoshnamvand, Mehdi,Huo, Can,Liu, Jingfu. Silver nanoparticles synthesized using Allium ampeloprasum L. leaf extract: Characterization and performance in catalytic reduction of 4-nitrophenol and antioxidant activity[J]. JOURNAL OF MOLECULAR STRUCTURE,2019,1175:90-96. |
APA | Khoshnamvand, Mehdi,Huo, Can,&Liu, Jingfu.(2019).Silver nanoparticles synthesized using Allium ampeloprasum L. leaf extract: Characterization and performance in catalytic reduction of 4-nitrophenol and antioxidant activity.JOURNAL OF MOLECULAR STRUCTURE,1175,90-96. |
MLA | Khoshnamvand, Mehdi,et al."Silver nanoparticles synthesized using Allium ampeloprasum L. leaf extract: Characterization and performance in catalytic reduction of 4-nitrophenol and antioxidant activity".JOURNAL OF MOLECULAR STRUCTURE 1175(2019):90-96. |
入库方式: OAI收割
来源:生态环境研究中心
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