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PPh3/I-2-catalyzed one-pot synthesis of 4,6-diarylpyrimidin-2(1H)-ones

文献类型：期刊论文

作者Zhang, Yanzhi1; Lei, Min4,5; Xue, Kangsheng2; Sun, Guoxiang2,3; Zhou, Yang4,5; Hou, Jinjun4,5; Long, Huali4,5; Zhang, Zijia4,5; Chen, Xubing1; Wu, Wanying4,5
刊名SYNTHETIC COMMUNICATIONS
出版日期2020-09-04
页码8
关键词46-diarylpyrimidin-2-(1H)-ones PPh3 I2 Aldehyde Ketone Biginelli reaction
ISSN号0039-7911
DOI10.1080/00397911.2020.1815784
通讯作者Chen, Xubing(abing780113@163.com) ; Wu, Wanying(wanyingwu@simm.ac.cn)
英文摘要A method using PPh3/I-2-catalyzed three-component Biginelli reaction of aromatic ketone, aromatic aldehyde and urea to synthesize4,6-diarylpyrimidin-2-(1H)-ones is described. Under the experimental conditions, the main reaction products are 4,6-diarylpyrimidin-2-(1H)-ones not 4,6-diaryl-3,4-dihydropyrimidin-2(1H)-ones. The advantage of this method is to achieve improved product yields with an inexpensive and readily available catalyst, and easy experimental set-up, which provides a good method to synthesize 4,6-diarylpyrimidin-2-(1H)-ones.
WOS关键词IMPROVED PROTOCOL CONDITIONS ; CALCIUM-CHANNEL BLOCKERS ; EFFICIENT CATALYST ; CONDENSATION REACTION ; BIGINELLI REACTION ; ACID-ESTERS ; DIHYDROPYRIMIDINONES ; 3,4-DIHYDROPYRIMIDIN-2(1H)-ONES ; CHLORIDE ; DERIVATIVES
资助项目Special Fund for Strategic Pilot Technology Chinese Academy of Sciences[XDA12020379] ; National Natural Science Foundation of China[81973455] ; National Key R&D Program of China[2018YFC1707900]
WOS研究方向Chemistry
语种英语
WOS记录号WOS:000567568800001
出版者TAYLOR & FRANCIS INC
源URL[http://119.78.100.183/handle/2S10ELR8/291044]  
专题中国科学院上海药物研究所
通讯作者Chen, Xubing; Wu, Wanying
作者单位1.Dali Univ, Coll Pharm, Dali, Peoples R China
2.Changchun Univ Chinese Med, Coll Pharm, Changchun, Peoples R China
3.Yancheng Inst Technol, Sch Chem & Chem Engn, Yancheng, Peoples R China
4.Chinese Acad Sci, Shanghai Res Ctr Modernizat Tradit Chinese Med, Shanghai Inst Mat Med, Natl Engn Lab TCM Standardizat Technol, Shanghai, Peoples R China
5.Univ Chinese Acad Sci, Beijing, Peoples R China
推荐引用方式
GB/T 7714		 Zhang, Yanzhi,Lei, Min,Xue, Kangsheng,et al. PPh3/I-2-catalyzed one-pot synthesis of 4,6-diarylpyrimidin-2(1H)-ones[J]. SYNTHETIC COMMUNICATIONS,2020:8.
APA Zhang, Yanzhi.,Lei, Min.,Xue, Kangsheng.,Sun, Guoxiang.,Zhou, Yang.,...&Wu, Wanying.(2020).PPh3/I-2-catalyzed one-pot synthesis of 4,6-diarylpyrimidin-2(1H)-ones.SYNTHETIC COMMUNICATIONS,8.
MLA Zhang, Yanzhi,et al."PPh3/I-2-catalyzed one-pot synthesis of 4,6-diarylpyrimidin-2(1H)-ones".SYNTHETIC COMMUNICATIONS (2020):8.

入库方式： OAI收割

来源：上海药物研究所

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